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ChemicalBook CAS DataBase List 9-methyl-2,8,10-triazabicyclo[4.4.0]deca-2,4,8,11-tetraen-7-one
28279-12-1

9-methyl-2,8,10-triazabicyclo[4.4.0]deca-2,4,8,11-tetraen-7-one synthesis

6synthesis methods
-

Yield:28279-12-1 86%

Reaction Conditions:

with acetic acid in ethanol at 110; for 12 h;Inert atmosphere;Sealed tube;

Steps:

3.2.2. Method 2

General procedure: The 2-aminobenzamide (1 equiv), the orthoester (2-3 equiv) and absolute ethanol (2-3 mL) wereplaced in a 15-mL Chemglass screw-cap pressure tube (No. CG-1880-01, Chemglass, Vineland, NJ,USA). Glacial acetic acid (3 equiv) was added, N2 was introduced to the vessel and the cap wastightened. The vessel was heated at 110 °C for 12-72 h, then cooled and concentrated to give thequinazolinone, which was purified by crystallization from absolute ethanol or trituration from 5%ether in pentane. The following compounds were prepared:

References:

Gavin, Joshua T.;Annor-Gyamfi, Joel K.;Bunce, Richard A. [Molecules,2018,vol. 23,# 11,art. no. 2925]

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