TRIETHYLAMINE HYDROBROMIDE synthesis
- Product Name:TRIETHYLAMINE HYDROBROMIDE
- CAS Number:636-70-4
- Molecular formula:C6H16BrN
- Molecular Weight:182.1
2576-47-8
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555-16-8
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![Ethanamine, 2-bromo-N-[(4-nitrophenyl)methylene]-](/CAS/20210305/GIF/524678-17-9.gif)
524678-17-9
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636-70-4
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Yield:524678-17-9 80%
Reaction Conditions:
with triethylamine in dichloromethane;
Steps:
11.a a) Protection of 2-bromoethylammonium bromide
14 mmol (2.87 g) of 2-bromoethylammonium bromide 1 and 14 mmol (1.95 ml, 1.42 g) of triethylamine are dissolved with stirring in 100 ml of dichloromethane in a 150 ml two-necked flask. 10 mmol (1.51 g) of para-nitrobenzaldehyde 2 are added to the solution and the mixture is kept stirred overnight. [0201] The solvent is evaporated and the resulting yellow solid is taken up in 50 ml of dichloromethane and 50 ml of water. The organic phase is extracted with 3×25 ml of dichloromethane and washed with 3×25 ml of water, then dried over magnesium sulphate and concentrated under vacuum. 2.16 g of yellow solid 3 are obtained. The yield is 80%
References:
US2005/8568,2005,A1 Location in patent:Page 8
590-97-6
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636-70-4
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121-44-8
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636-70-4
130 suppliers
$36.22/100g