PHENYL PROPARGYL ETHER synthesis
- Product Name:PHENYL PROPARGYL ETHER
- CAS Number:13045-88-0
- Molecular formula:C9H8O
- Molecular Weight:132.16
![Benzene, [(1,2-dichloroethenyl)oxy]-](/CAS/20210305/GIF/89894-42-8.gif)
Yield:13045-88-0 78 %
Reaction Conditions:
Stage #1: 1,2-dichlorovinyl phenyl etherwith n-butyllithium in tetrahydrofuran at -78;Inert atmosphere;
Stage #2: methyl iodide in tetrahydrofuran at -78 - 20;Inert atmosphere;
References:
Coles-Taylor, Brandon L.;Ellinwood, Mitchell L.;McCallum, Maximilian S.;McCormack, Sara L.;Jones, Meredith H.;Mu?oz, Andrés G.;Michel, Brian W. [Journal of Organic Chemistry,2022,vol. 87,# 24,p. 16517 - 16525] Location in patent:supporting information
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