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81787-92-0

methyl 1-benzyl-1H-indole-2-carboxylate synthesis

5synthesis methods
-

Yield:81787-92-0 99.3%

Reaction Conditions:

Stage #1: indole-2-carboxylic acid methyl esterwith sodium hydride in N,N-dimethyl-formamide at 20; for 1 h;Metallation;
Stage #2: benzyl bromide in N,N-dimethyl-formamide at 20; for 5 h;Alkylation;

References:

Kitano, Masafumi;Kojima, Atsuyuki;Nakano, Kazuhiro;Miyagishi, Akira;Noguchi, Tsuyoshi;Ohashi, Naohito [Chemical and Pharmaceutical Bulletin,1999,vol. 47,# 11,p. 1538 - 1548]