GLYCERYL TRIMETHACRYLATE synthesis
- Product Name:GLYCERYL TRIMETHACRYLATE
- CAS Number:7401-88-9
- Molecular formula:C15H20O6
- Molecular Weight:296.32
1830-78-0
96 suppliers
$14.00/5g
7401-88-9
12 suppliers
$505.12/5MG
Yield: 32%
Reaction Conditions:
with sodium hydride in hexane at 20;Solvent;
Steps:
2 Example 2
Sodium hydride (3.05 g, 70 mmol) 55% in liquid paraffin was subjected to cleaning with hexane, and the liquid paraffin was removed. After removing the liquid paraffin, 150 mL of hexane was added to sodium hydride at room temperature and stirred. Then, glycerin-1,3-dimethacrylate (15.98 g, 70 mmol) was slowly dripped into the above-described mixture of sodium hydride and hexane at room temperature. Then, precipitated 10.8 g of white solid precipitate was removed by filtration. Next, by employing a rotary evaporator, hexane was removed from the filtrate (i.e., the mixture of sodium hydride, hexane, and glycerin-1,3-dimethacrylate after filtration). Accordingly, glycerin trimethacrylate as shown in <
References:
MORITA, Mitsunobu;NOGUCHI, Soh;MIKI, Daisuke US2016/23984, 2016, A1 Location in patent:Paragraph 0025
56-81-5
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$5.00/25g
920-46-7
340 suppliers
$20.00/1g
7401-88-9
12 suppliers
$505.12/5MG
80-62-6
618 suppliers
$18.00/25mL
56-81-5
1688 suppliers
$5.00/25g
7401-88-9
12 suppliers
$505.12/5MG
79-41-4
524 suppliers
$14.00/5g
56-81-5
1688 suppliers
$5.00/25g
7401-88-9
12 suppliers
$505.12/5MG
5919-74-4
105 suppliers
$35.00/1 g
1830-78-0
96 suppliers
$14.00/5g