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ChemicalBook CAS DataBase List CHLOROTRIBENZYLSILANE
18740-59-5

CHLOROTRIBENZYLSILANE synthesis

10synthesis methods
It is prepared by reaction of benzylmagnesium chloride with SiCl4 in ether; separation from mono- and dibenzylated chlorosilane byproducts is then accomplished by fractional distillation (boiling range 300–360 °C/100 mmHg). Other preparations involve the chlorination of tribenzylsilane using Cl2 or an acyl chloride. No yields are reported for any of the above preparative procedures.
-

Yield:-

Reaction Conditions:

with tetrachloromethane;chlorine

References:

Jenkins;Post [Journal of Organic Chemistry,1950,vol. 15,p. 552,554]

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