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ChemicalBook CAS DataBase List 4-METHYLFORMANILIDE
3085-54-9

4-METHYLFORMANILIDE synthesis

11synthesis methods
-

Yield:3085-54-9 89%

Reaction Conditions:

with oxygen in acetonitrile at 60; for 24 h;Green chemistry;

Steps:


General procedure: To a mixture of p-methoxyaniline (1a, 0.5 mmol) and cyclohexanecarboxaldehyde(2e, 0.6 mmol), and CH3CN (1.5 mL) in a 25ml round-bottomed flask at 60°C underair, the reaction vessel was allowed to stir at 60 °C for 24 h. After reaction, theresulting mixture was isolated by column chromatography on silica gel withEtOAc/petroleum (1:2) to obtain the products(3a) as brown solid. The compounds(3b-3n) were obtained by the same method.

References:

Qin, Yuancheng;Cheng, Yuanyuan;Luo, Xubiao;Li, Mingjun;Xie, Yu;Gao, Yunhua [Synlett,2015,vol. 26,# 13,art. no. ST-2015-W0292-L,p. 1900 - 1904] Location in patent:supporting information

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