2-METHYLBENZO[B]THIOPHENE synthesis
- Product Name:2-METHYLBENZO[B]THIOPHENE
- CAS Number:1195-14-8
- Molecular formula:C9H8S
- Molecular Weight:148.22
77-78-1
319 suppliers
$19.69/1ml
95-15-8
380 suppliers
$6.00/5g
1195-14-8
104 suppliers
$16.00/100mg
Yield: 82%
Reaction Conditions:
Stage #1:Benzo[b]thiophene with n-butyllithium in diethyl ether;hexane at -78; for 0.5 h;Inert atmosphere;
Stage #2:dimethyl sulfate in diethyl ether;hexane at -78; for 0.5 h;Inert atmosphere;
References:
Tosatti, Paolo;Pfaltz, Andreas [Angewandte Chemie - International Edition,2017,vol. 56,# 16,p. 4579 - 4582][Angew. Chem.,2017,vol. 129,p. 4650 - 4653,4] Location in patent:supporting information
95-15-8
380 suppliers
$6.00/5g
74-88-4
351 suppliers
$15.00/10g
1195-14-8
104 suppliers
$16.00/100mg
![2-BENZO[B]THIOPHENE-2-BORONIC ACID PINACOL ESTER](/CAS/GIF/376584-76-8.gif)
376584-76-8
61 suppliers
$67.00/1g
74-88-4
351 suppliers
$15.00/10g
1195-14-8
104 suppliers
$16.00/100mg
13061-96-6
306 suppliers
$6.00/1g
![Benzo[b]thiophene-2-carboxamide,N-phenyl-](/CAS/20180529/GIF/6314-40-5.gif)
6314-40-5
8 suppliers
inquiry
1195-14-8
104 suppliers
$16.00/100mg
554-14-3
263 suppliers
$6.00/5g
696-59-3
401 suppliers
$7.00/25g
1195-14-8
104 suppliers
$16.00/100mg