2-Bromo-4-fluoroaniline synthesis
- Product Name:2-Bromo-4-fluoroaniline
- CAS Number:1003-98-1
- Molecular formula:C6H5BrFN
- Molecular Weight:190.01
371-40-4
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1003-98-1
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Yield:1003-98-1 95%
Reaction Conditions:
with N-Bromosuccinimide in N,N-dimethyl-formamide;
Steps:
3.1.1-5
Add 200 mL distilled DMF and 4-fluoroaniline (8.64 mL, 58.13 mmol) to a two neck flask. Slowly dropwise N-Bromosuccinimide (11.4 g, 63.95 mmol) dissolved in DMF. When the reaction is complete, extract with CH2Cl2. Purification by column separation (EA: Hx = 1: 4) (yield: 95%)
References:
KR2018/50795,2018,A Location in patent:Paragraph 0134; 0135; 0152-0154
700-36-7
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1003-98-1
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1009-22-9
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1003-98-1
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351-83-7
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1003-98-1
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