2-(4'-Piperidinyl) pyridine synthesis
- Product Name:2-(4'-Piperidinyl) pyridine
- CAS Number:30532-37-7
- Molecular formula:C10H14N2
- Molecular Weight:162.23
![[2,4'-Bipyridine]-1'(2'H)-carboxylic acid, 3',6'-dihydro-, phenylmethyl ester](/CAS/20210305/GIF/161610-17-9.gif)
161610-17-9
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30532-37-7
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Yield:30532-37-7 88%
Reaction Conditions:
with hydrogen;10% Pd/C at 50; under 3102.97 Torr; for 40 h;
Steps:
36C EXAMPLE 36C; 2-(4-piperidinyl)pyridine
The product from Example 36B was treated with 10% Pd/C (250 mg) at 60 psi and 50° C. for 40 hours to provide the title compound (150 mg, 88% yield). MS (DCI/NH3) m/e 163 (M+H)+.
References:
US2003/229094,2003,A1 Location in patent:Page 73
143924-45-2
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![3',4',5',6'-tetrahydro-2'H-[2,4'-bipyridine]-1'-carboxylic acid tert-butyl ester](/CAS/GIF/206446-49-3.gif)
206446-49-3
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30532-37-7
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102325-51-9
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1121-89-7
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7732-18-5
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30532-37-7
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