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New Journal of Chemistry

New Journal of Chemistry

IF: 2.7
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Radical synthesis of trialkyl, triaryl, trisilyl and tristannyl phosphines from P4??

Published:13 April 2010 DOI: 10.1039/C0NJ00124D
Brandi M. Cossairt and Christopher C. Cummins

Abstract

A reaction scheme has been devised according to 3 RX + 3 Ti(III) + 0.25 P4 → PR3 + 3 XTi(IV), wherein RX = PhBr, CyBr, Me3SiI or Ph3SnCl, with contrasting results in the case of more hindered RX. The scheme accomplishes the direct radical functionalization of white phosphorus without the intermediacy of PCl3.

Substances (7)

Related products
Procduct Name CAS Molecular Formula Supplier Price
Pyridine hydrobromide 18820-82-1 C5H5N.BrH 368 suppliers $5.00-$4306.35
Phosphorus trichloride 7719-12-2 Cl3P 136 suppliers $30.30-$762.00
ANTIMONY (III) TELLURIDE 1327-50-0 Sb2Te3 115 suppliers $29.00-$643.65
DYNAMIN INHIBITORY PEPTIDE 251634-21-6 C47H80N18O14 50 suppliers $120.00-$840.00
Cybr antibody 12 suppliers Inquiry
CaM Kinase IV 8 suppliers Inquiry
CANCA 22541-14-6 H2Pr+3 8 suppliers Inquiry

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