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95-03-4

4-氯-2-氨基苯甲醚(95-03-4)核磁圖(¹HNMR)

產(chǎn)品名稱:4-氯-2-氨基苯甲醚

CAS:95-03-4

分子式:C7H8ClNO

分子量: 157.6

InChI:InChI=1S/C7H8ClNO/c1-10-7-3-2-5(8)4-6(7)9/h2-4H,9H2,1H3

InChIKey: WBSMIPLNPSCJFS-UHFFFAOYSA-N

Smiles:C1(N)=CC(Cl)=CC=C1OC

Mass

MS-NW-7089          
5-chloro-o-anisidine
C7H8ClNO            (Mass of molecular ion:    157)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.1
      27.0       1.2
      28.0       5.4
      37.0       1.7
      38.0       2.9
      38.5       2.5
      39.0       3.1
      39.5       1.7
      41.0       1.6
      49.0       1.4
      50.0       4.7
      51.0      13.6
      52.0      10.4
      53.0       3.2
      54.0       1.1
      61.0       1.9
      62.0       2.9
      63.0       6.2
      64.0       2.1
      65.0       3.0
      73.0       2.7
      75.0       1.6
      76.0       2.7
      77.0       1.5
      78.0      12.2
      79.0       4.7
      86.0       1.0
      87.0       4.2
      88.0       1.0
      89.0       1.9
      90.0       3.4
      91.0       1.4
      92.0       1.2
      93.0       3.8
      99.0       4.3
     101.0       1.3
     114.0      44.7
     115.0       3.6
     116.0      14.4
     117.0       1.2
     126.0       2.2
     127.0       1.0
     128.0       1.2
     142.0     100.0
     143.0       7.5
     144.0      32.1
     145.0       2.5
     157.0      66.6
     158.0       6.0
     159.0      21.8
     160.0       2.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₇ H₈ Cl N O	0.043 g : 0.5 ml CDCl₃
5-chloro-o-anisidine

    Assign.     Shift(ppm)

      A             6.64
      B             3.794
      C             3.77

     Hz     ppm     Int.

    595.00   6.644   1000
    339.81   3.795    992
    334.88   3.740     95

in CDCl3

CCl4 solution

KBr disc

nujol mull

4880 A,200 M,powder

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4-氯-2-氨基苯甲醚(95-03-4)核磁圖(1HNMR)

4-氯-2-氨基苯甲醚(95-03-4)核磁圖(¹HNMR)