1-萘氨基苯(90-30-2)紅外圖譜(IR2)

產(chǎn)品名稱:1-萘氨基苯

CAS:90-30-2

分子式:C16H13N

分子量: 219.28

InChI:InChI=1S/C16H13N/c1-2-9-14(10-3-1)17-16-12-6-8-13-7-4-5-11-15(13)16/h1-12,17H

InChIKey: XQVWYOYUZDUNRW-UHFFFAOYSA-N

Smiles:C1(NC2=CC=CC=C2)=C2C(C=CC=C2)=CC=C1

Mass

MS-NW-0675          
N-phenyl-1-naphthylamine
C16H13N             (Mass of molecular ion:    219)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      39.0       1.9
      50.0       1.1
      51.0       3.7
      63.0       2.0
      65.0       1.3
      75.0       1.5
      77.0       3.7
      89.0       1.7
      94.5       1.9
      95.5       3.1
      96.5       1.8
     101.0       1.3
     102.0       3.2
     107.0       1.8
     107.5       1.1
     108.0       1.4
     108.5      18.9
     109.0       5.6
     109.5       6.9
     110.0       1.3
     115.0       8.5
     116.0       3.2
     126.0       2.0
     127.0       3.3
     128.0       1.2
     140.0       1.3
     153.0       1.9
     165.0       1.1
     189.0       2.0
     190.0       1.5
     191.0       1.5
     204.0       3.1
     215.0       1.3
     216.0       7.4
     217.0      31.4
     218.0      42.1
     219.0     100.0
     220.0      17.3
     221.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₆ H₁₃ N	0.050 g : 0.5 ml CDCl₃
N-phenyl-1-naphthylamine

    Assign.     Shift(ppm)

      A             7.958
      B             7.821
      C             7.526
      D             7.45
      E             7.42
      F             7.340
      G             7.33
      J             7.216
      K             6.936
      L             6.882
      M             5.84
     
     ASSIGNED BY H-H AND C-H COSY.

     Hz     ppm     Int.

   3184.81   7.969    334
   3176.64   7.949    368
   3130.25   7.833    313
   3128.91   7.830    342
   3121.46   7.811    367
   3011.35   7.535    288
   3004.03   7.517    344
   2996.58   7.499     35
   2996.09   7.497     34
   2986.33   7.473    148
   2985.11   7.470    170
   2979.49   7.456    339
   2978.39   7.453    351
   2971.80   7.437    370
   2970.09   7.432    534
   2968.38   7.428    370
   2961.67   7.411    352
   2960.45   7.408    313
   2954.96   7.394    164
   2953.61   7.391    148
   2949.46   7.381     38
   2944.46   7.368    207
   2937.01   7.349    565
   2929.57   7.331   1000
   2927.73   7.326    659
   2922.00   7.312    190
   2920.29   7.308    129
   2892.33   7.238    407
   2884.77   7.219    694
   2883.91   7.217    714
   2876.46   7.198    522
   2775.63   6.946    775
   2767.94   6.926    667
   2757.20   6.900    264
   2749.88   6.881    433
   2742.55   6.863    209
   2334.23   5.841    258

in CDCl3