1,1,3,3-四甲基-1,3-二乙烯基二硅氮烷(7691-02-3)質(zhì)譜(MS)

產(chǎn)品名稱:1,1,3,3-四甲基-1,3-二乙烯基二硅氮烷

CAS:7691-02-3

分子式:C8H19NSi2

分子量: 185.41

InChI:InChI=1S/C8H19NSi2/c1-7-10(3,4)9-11(5,6)8-2/h7-9H,1-2H2,3-6H3

InChIKey: WYUIWUCVZCRTRH-UHFFFAOYSA-N

Smiles:[Si](C=C)(C)(C)N[Si](C=C)(C)C

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-6665          
1,1,3,3-tetramethyl-1,3-divinyldisilazane
C8H19NSi2           (Mass of molecular ion:    185)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      28.0       1.3
      31.0       1.4
      43.0       3.9
      44.0       1.7
      45.0       4.5
      50.5       1.5
      51.5       3.1
      55.0       1.2
      57.5       2.8
      58.0       1.2
      58.5       5.7
      59.0      14.8
      60.0       4.4
      61.0       1.4
      63.5       7.1
      64.0       1.6
      64.5       4.8
      65.0       1.0
      70.0       2.6
      71.0       2.7
      71.5       1.1
      72.0       1.5
      73.0      13.4
      74.0       9.2
      75.0       1.5
      77.5       3.2
      83.0       1.2
      85.0       5.1
      86.0       4.0
      87.0       2.1
      99.0       1.0
     100.0       7.6
     101.0       1.1
     102.0       6.4
     103.0       1.2
     104.0       1.0
     112.0       1.3
     114.0       1.4
     116.0      26.5
     117.0       5.7
     118.0       5.8
     119.0       1.2
     128.0       7.8
     129.0       1.6
     130.0      16.8
     131.0       2.8
     132.0       3.2
     142.0      40.7
     143.0       7.7
     144.0       5.6
     145.0       1.1
     153.0       1.1
     154.0       2.8
     156.0       1.2
     158.0      15.2
     159.0       3.2
     160.0       1.4
     168.0       2.9
     170.0     100.0
     171.0      21.2
     172.0       8.6
     173.0       1.2
     185.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₉ N Si₂	0.05 ml : 0.5 ml CDCl₃
1,1,3,3-tetramethyl-1,3-divinyldisilazane

    Assign.     Shift(ppm)

      A             6.140
      B             5.906
      C             5.697
      D             0.126

     Hz     ppm     Int.

   2473.51   6.190    133
   2458.74   6.153    173
   2453.25   6.139    163
   2438.60   6.102    214
   2368.90   5.928    201
   2364.87   5.918    223
   2354.25   5.891    165
   2350.22   5.881    167
   2288.09   5.726    200
   2284.18   5.716    187
   2267.94   5.675    166
   2263.92   5.665    157
     62.01   0.156     25
     61.28   0.154     24
     53.96   0.136    202
     50.42   0.127   1000
     47.12   0.118    291
     40.28   0.101     55

in CDCl3