1-溴金剛烷(768-90-1)核磁圖(1HNMR)
InChI:InChI=1S/C10H15Br/c11-10-4-7-1-8(5-10)3-9(2-7)6-10/h7-9H,1-6H2
InChIKey: VQHPRVYDKRESCL-UHFFFAOYSA-N
Smiles:C12(Br)CC3CC(CC(C3)C1)C2
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Mass
MS-KW-0260
1-bromotricyclo(3.3.1.1(3,7))decane
C10H15Br (Mass of molecular ion: 214)
Source Temperature: 230 °C
Sample Temperature: 150 °C
Reservoir, 75 eV
27.0 2.8
29.0 1.4
39.0 5.6
41.0 6.0
43.0 1.0
51.0 1.9
52.0 1.1
53.0 3.1
55.0 4.3
65.0 3.5
66.0 1.6
67.0 7.7
69.0 2.1
77.0 6.6
78.0 2.4
79.0 20.3
80.0 2.0
81.0 6.0
91.0 5.8
92.0 2.0
93.0 16.6
94.0 2.0
95.0 4.5
105.0 1.2
107.0 5.8
135.0 100.0
136.0 11.3
152.0 1.0
400 MHz in CDCl3
90 MHz in CDCl3
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| 1H NMR |
399.65 MHz |
| C10H15Br
|
0.040 g : 0.5 ml CDCl3
|
| 1-bromoadamantane
|
 |
Assign. Shift(ppm)
A 2.367
B 2.104
C 1.73
|
Hz ppm Int.
947.51 2.371 1000
944.22 2.362 971
841.07 2.104 284
694.95 1.739 683
691.90 1.731 964
688.48 1.723 563
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| 1H NMR |
89.56 MHz |
| C10 H15 Br
|
0.046 g : 0.5 ml CDCl3
|
| 1-bromotricyclo(3.3.1.1(3,7))decane
|
|
Assign. Shift(ppm)
A 2.363
B 2.10
C 1.73
J(A,B)=3.0HZ. J(B,C)=3.0HZ.
|
Hz ppm Int.
213.38 2.383 768
210.38 2.350 1000
200.81 2.243 50
188.25 2.102 263
157.88 1.763 578
155.00 1.731 871
151.94 1.697 471