11-苯氧基十一烷酸(7170-44-7)核磁圖(¹HNMR)

產(chǎn)品名稱:11-苯氧基十一烷酸

CAS:7170-44-7

分子式:C17H26O3

分子量: 278.39

Mass

MS-IW-0711          
11-phenoxyundecanoic acid
C17H26O3            (Mass of molecular ion:    278)

   Source Temperature: 170 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       2.1
      41.0       3.4
      43.0       2.9
      55.0       6.6
      57.0       1.6
      67.0       1.2
      69.0       5.3
      71.0       1.0
      77.0       2.2
      81.0       1.6
      82.0       1.0
      83.0       4.1
      84.0       1.2
      94.0     100.0
      95.0       8.4
      96.0       1.2
      97.0       2.0
     107.0       1.4
     111.0       1.1
     149.0       2.4
     167.0       2.4
     278.0      16.6
     279.0       3.2
     292.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₇ H₂₆ O₃	0.038 g : 0.5 ml CDCl₃
11-phenoxyundecanoic acid

    Assign.     Shift(ppm)

      A            11.
      B             7.266
      C             6.92
      D             6.89
      E             3.941
      F             2.341
      G             1.77
      J             1.63
      K             1.45
      L             1.34
      M             1.30

     Hz     ppm     Int.

   2915.28   7.295     43
   2912.90   7.289    348
   2910.70   7.284    120
   2907.95   7.277     67
   2905.39   7.270    483
   2904.10   7.267    465
   2901.91   7.262     74
   2898.79   7.254    153
   2896.78   7.249    433
   2894.40   7.243    182
   2774.06   6.942    102
   2773.14   6.939    187
   2772.04   6.937    122
   2765.81   6.921    338
   2764.90   6.919    201
   2761.42   6.910     95
   2759.22   6.905    554
   2758.30   6.902    647
   2756.11   6.897    148
   2754.46   6.893     48
   2752.44   6.888    171
   2751.53   6.885    272
   2750.43   6.883    507
   2749.51   6.880    378
   2746.95   6.874     60
   1582.01   3.959    400
   1575.42   3.943    832
   1569.00   3.926    417
    943.86   2.362    215
    936.35   2.343    403
    928.84   2.325    241
    721.68   1.806     78
    715.08   1.790    225
    708.12   1.772    262
    706.84   1.769    210
    700.06   1.752    251
    693.47   1.736    104
    664.89   1.664     40
    663.25   1.660     38
    657.57   1.646    133
    650.42   1.628    209
    643.28   1.610    172
    635.95   1.592     70
    592.54   1.483     42
    591.99   1.482     41
    590.53   1.478     38
    585.40   1.465    115
    584.12   1.462    109
    578.44   1.448    178
    570.56   1.428    147
    565.80   1.416     52
    563.60   1.411     74
    520.38   1.303   1000

in CDCl3