N-芐基甲酰胺(6343-54-0)核磁圖(1HNMR)
InChI:
InChIKey:
Smiles:
-
Mass
MS-IW-0762
N-benzylformamide
C8H9NO (Mass of molecular ion: 135)
Source Temperature: 180 °C
Sample Temperature: 160 °C
Direct, 75 eV
27.0 2.1
28.0 10.9
29.0 2.2
30.0 4.7
39.0 5.1
41.0 3.3
42.0 1.4
43.0 3.1
44.0 1.3
50.0 2.9
51.0 7.3
52.0 2.2
53.0 1.9
55.0 2.5
56.0 1.4
57.0 4.6
58.0 2.2
63.0 2.9
65.0 7.4
70.0 2.1
77.0 12.2
78.0 5.7
79.0 24.8
80.0 2.1
87.0 3.6
89.0 5.6
90.0 5.4
91.0 30.8
92.0 8.8
104.0 3.3
105.0 1.1
106.0 24.2
107.0 6.3
108.0 1.1
116.0 2.7
117.0 1.7
118.0 4.9
134.0 43.9
135.0 100.0
136.0 10.5
400 MHz in CDCl3
400 MHz in DMSO-d6
-
| 1H NMR |
399.65 MHz |
| C8 H9 N O
|
0.05 ml : 0.5 ml CDCl3
|
| N-benzylformamide
|
 |
Assign. Shift(ppm)
A 8.465
B 7.406
C 7.268
D 7.167
E 3.305
|
Hz ppm Int.
3383.18 8.466 310
2969.48 7.431 52
2967.77 7.426 157
2965.45 7.421 72
2962.28 7.413 52
2961.18 7.410 107
2960.21 7.408 299
2959.23 7.405 259
2953.49 7.391 106
2951.78 7.386 261
2949.46 7.381 59
2912.11 7.287 78
2911.01 7.284 140
2909.79 7.281 85
2905.15 7.270 70
2903.69 7.266 193
2901.86 7.262 64
2897.22 7.250 51
2896.12 7.247 87
2894.90 7.244 49
2870.61 7.183 78
2869.26 7.180 277
2867.92 7.177 340
2865.72 7.171 94
2862.43 7.163 104
2861.69 7.161 151
2860.47 7.158 274
2859.38 7.155 235
2856.93 7.149 40
1321.04 3.306 1000
1320.43 3.304 908
-
| 1H NMR |
399.65 MHz |
| C8 H9 N O
|
0.036 g : 0.5 ml DMSO-d6
|
| N-benzylformamide
|
|
Assign. Shift(ppm)
A 8.52
B 8.150
C 7.327
D 7.27
E 7.25
F 4.311
|
Hz ppm Int.
3404.24 8.519 81
3258.21 8.153 591
3257.45 8.151 572
3256.53 8.149 566
2945.40 7.370 40
2940.06 7.357 31
2937.47 7.351 265
2936.40 7.348 331
2934.88 7.344 125
2933.20 7.340 55
2929.99 7.332 614
2929.23 7.330 758
2928.16 7.327 544
2924.04 7.317 282
2922.06 7.312 853
2915.65 7.296 37
2910.61 7.283 724
2909.24 7.280 1000
2908.78 7.279 976
2906.49 7.273 234
2902.07 7.262 682
2901.46 7.261 588
2897.95 7.252 215
2895.81 7.246 427
2893.22 7.240 112
2890.17 7.232 106
2888.64 7.228 157
2887.12 7.225 81
1726.23 4.320 989
1719.97 4.304 985