3-(4-甲氧基苯氧基)苯甲醛(62373-80-2)質(zhì)譜(MS)

產(chǎn)品名稱:3-(4-甲氧基苯氧基)苯甲醛

CAS:62373-80-2

分子式:C14H12O3

分子量: 228.24

Mass

MS-NW-7483          
m-(p-methoxyphenoxy)benzaldehyde
C14H12O3            (Mass of molecular ion:    228)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.3
      18.0       1.5
      26.0       1.2
      27.0       1.8
      28.0       5.4
      29.0       1.6
      38.0       2.5
      39.0       3.5
      41.0       4.2
      50.0       6.2
      51.0      16.3
      52.0       3.5
      53.0       1.8
      54.0       1.7
      55.0       3.1
      58.0       1.1
      59.0       1.8
      62.0       1.7
      63.0       6.6
      64.0       6.4
      65.0       2.8
      74.0       1.9
      75.0       2.6
      76.0       6.4
      77.0      25.6
      78.0       2.4
      79.0       1.4
      80.0       1.7
      91.0       1.4
      92.0       4.9
      95.0       4.7
     102.0       1.1
     105.0      19.5
     106.0       2.1
     109.0       1.2
     113.5       1.9
     115.0       2.2
     123.0      10.4
     124.0       1.5
     127.0       2.5
     128.0       5.8
     129.0      11.5
     130.0       1.3
     131.0       1.1
     139.0       1.3
     141.0       1.9
     155.0       1.0
     156.0       1.1
     157.0       8.1
     158.0       1.2
     168.0       1.0
     169.0       1.0
     171.0       2.0
     184.0       1.1
     185.0       5.7
     199.0       2.3
     211.0       1.0
     213.0      31.0
     214.0       6.0
     215.0       1.1
     227.0       1.8
     228.0     100.0
     229.0      15.5
     230.0       2.0
     258.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₂ O₃	0.05 ml : 0.5 ml CDCl₃
m-(p-methoxyphenoxy)benzaldehyde

    Assign.     Shift(ppm)

      A             9.900
      B             7.519
      C             7.434
      D             7.371
      E             7.213
      F             6.983
      G             6.896
      J             3.783

     Hz     ppm     Int.

   3956.45   9.900    458
   3010.71   7.534     70
   3009.49   7.531    113
   3008.12   7.527     74
   3003.23   7.515    105
   3001.86   7.512    165
   3000.64   7.509    105
   2978.82   7.454    121
   2971.04   7.435    173
   2963.10   7.415     98
   2947.85   7.377    133
   2946.47   7.373    135
   2945.25   7.370    149
   2943.88   7.367    131
   2888.18   7.227     97
   2887.12   7.225    101
   2885.44   7.220     91
   2884.52   7.218     89
   2879.94   7.207     83
   2878.88   7.204     82
   2877.35   7.200     79
   2876.28   7.197     72
   2799.99   7.007     33
   2796.48   6.998    268
   2794.04   6.992    105
   2789.76   6.981    134
   2787.32   6.975    417
   2783.81   6.966     56
   2763.21   6.915     62
   2759.86   6.906    408
   2757.26   6.900    123
   2752.99   6.889    104
   2750.70   6.883    254
   1511.84   3.783   1000

in CDCl3