叔丁基二苯基氯硅烷(58479-61-1)核磁圖(¹HNMR)

產(chǎn)品名稱:叔丁基二苯基氯硅烷

CAS:58479-61-1

分子式:C16H19ClSi

分子量: 274.86

InChI:InChI=1S/C16H19ClSi/c1-16(2,3)18(17,14-10-6-4-7-11-14)15-12-8-5-9-13-15/h4-13H,1-3H3

InChIKey: MHYGQXWCZAYSLJ-UHFFFAOYSA-N

Smiles:[Si](C1=CC=CC=C1)(C1=CC=CC=C1)(Cl)C(C)(C)C

Mass

MS-NW-7372          
tert-butylchlorodiphenylsilane
C16H19ClSi          (Mass of molecular ion:    274)

   Source Temperature: 220 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      29.0       2.2
      39.0       1.6
      41.0       3.1
      51.0       3.1
      53.0       2.0
      57.0       2.2
      63.0      14.5
      65.0       5.5
      77.0       2.2
      79.0       1.0
      91.0       1.3
     103.0       1.3
     105.0       3.0
     129.0       1.3
     139.0       2.0
     140.0       4.2
     141.0       2.3
     142.0       1.7
     152.0       2.5
     153.0       1.1
     155.0       5.1
     165.0       1.0
     180.0       3.3
     181.0      11.9
     182.0       2.4
     199.0       1.3
     215.0       2.9
     217.0     100.0
     218.0      18.5
     219.0      36.9
     220.0       6.5
     221.0       1.7
     274.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₆ H₁₉ Cl Si	0.05 ml : 0.5 ml CDCl₃
tert-butylchlorodiphenylsilane

    Assign.     Shift(ppm)

      A             7.757
      B             7.41
      C             7.37
      D             1.134

     Hz     ppm     Int.

   3104.98   7.770    138
   3103.52   7.766    160
   3101.93   7.762     71
   3099.24   7.755     55
   3097.17   7.750    157
   3095.46   7.746    148
   2961.67   7.411     80
   2958.74   7.404     34
   2956.42   7.398     73
   2954.71   7.394    121
   2952.88   7.389     86
   2951.42   7.386    127
   2950.93   7.384    143
   2949.46   7.381     75
   2945.07   7.370     91
   2943.73   7.366    150
   2941.65   7.361     39
   2937.13   7.350     57
   2935.06   7.345     41
    456.54   1.143    105
    453.37   1.135   1000
    449.58   1.125     64

in CDCl3