N-甲基-1-萘胺鹽酸鹽(4643-36-1)核磁圖(¹HNMR)

產(chǎn)品名稱:N-甲基-1-萘胺鹽酸鹽

CAS:4643-36-1

分子式:C11H12ClN

分子量: 193.67

InChI:InChI=1S/C11H11N.ClH/c1-12-11-8-4-6-9-5-2-3-7-10(9)11;/h2-8,12H,1H3;1H

InChIKey: ALZGTEASAJRPTL-UHFFFAOYSA-N

Smiles:C12C=CC=CC=1C=CC=C2NC.Cl

Mass

MS-IW-7455          
N-methyl-1-naphthylamine hydrochloride
C11H11N HCl         (Mass of molecular ion:    157)

   Source Temperature: 120 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      36.0       8.5
      38.0       2.9
      51.0       1.7
      63.0       2.8
      64.0       1.5
      65.0       2.5
      74.0       1.2
      75.0       1.6
      76.0       1.0
      76.5       2.1
      77.0       6.2
      77.5       7.4
      78.0       4.1
      78.5       5.2
      89.0       1.7
     101.0       1.5
     113.0       1.1
     114.0       1.4
     115.0      19.4
     116.0       3.0
     126.0       3.0
     127.0       7.9
     128.0      16.6
     129.0      17.4
     130.0       3.0
     140.0       1.7
     141.0       1.0
     142.0       5.6
     154.0       6.1
     155.0       3.2
     156.0      38.4
     157.0     100.0
     158.0      12.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₁ N	0.040 g : 0.5 ml CDCl₃
N-methyl-1-naphthylamine hydrochloride

    Assign.     Shift(ppm)

      A            12.0
      B             8.456
      C             7.992
      D             7.908
      E             7.896
      F             7.694
      G             7.578
      J             7.467
      K             3.244

     Hz     ppm     Int.

   4789.07  11.984     30
   3384.37   8.469     88
   3383.63   8.467     93
   3375.94   8.448     95
   3375.03   8.445     99
   3198.45   8.004    103
   3197.54   8.001    121
   3191.13   7.985    119
   3190.03   7.983    127
   3165.30   7.921     91
   3160.35   7.908    105
   3157.06   7.900    110
   3156.69   7.899    104
   3151.93   7.887    114
   3083.79   7.717     50
   3082.51   7.714     54
   3076.83   7.699     72
   3075.37   7.696     99
   3074.08   7.692     57
   3068.22   7.678     66
   3067.12   7.675     65
   3035.98   7.597     70
   3035.07   7.595     76
   3029.02   7.580     61
   3027.93   7.577    105
   3026.83   7.574     76
   3020.78   7.559     51
   3019.87   7.557     52
   2992.02   7.487    116
   2984.51   7.468    123
   2983.78   7.466    128
   2976.27   7.448    102
   1296.82   3.245   1000

in CDCl3