氯甲酸對(duì)硝基芐酯(4457-32-3)核磁圖(¹HNMR)

產(chǎn)品名稱:氯甲酸對(duì)硝基芐酯

CAS:4457-32-3

分子式:C8H6ClNO4

分子量: 215.59

Mass

MS-NW-7976          
p-nitrobenzyl chloroformate
C8H6ClNO4           (Mass of molecular ion:    215)

   Source Temperature: 150 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      18.0       1.4
      27.0       3.1
      28.0       4.2
      29.0       3.1
      30.0      52.0
      36.0       1.6
      37.0       1.4
      38.0       3.9
      39.0      12.2
      40.0       2.1
      44.0       4.5
      50.0       9.7
      51.0      16.2
      52.0       4.6
      61.0       1.1
      62.0       4.2
      63.0      18.4
      64.0       6.1
      65.0       5.7
      66.0       1.0
      74.0       2.4
      75.0       3.9
      76.0       5.0
      77.0      15.9
      78.0      25.9
      79.0       2.2
      89.0      77.1
      90.0      20.2
      91.0       1.6
      92.0       1.1
      94.0       1.0
      99.0       2.3
     104.0       1.5
     105.0       3.7
     106.0      17.8
     107.0       1.8
     113.0       1.4
     124.0       1.8
     125.0       9.2
     126.0       1.2
     127.0       3.2
     135.0      11.9
     136.0     100.0
     137.0       8.3
     141.0       3.3
     143.0       1.3
     152.0       4.4
     154.0       2.2
     169.0       2.2
     171.0       7.1
     173.0       2.1
     179.0       1.1
     199.0       3.1
     215.0      33.7
     216.0       4.7
     217.0      11.1
     218.0       1.6

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₆ Cl N O₄	0.05 ml : 0.5 ml CDCl₃
p-nitrobenzyl chloroformate

    Assign.     Shift(ppm)

      A             8.255
      B             7.601
      C             5.430

     Hz     ppm     Int.

   3306.27   8.273     91
   3303.96   8.268    527
   3302.00   8.263    203
   3297.12   8.251    191
   3295.17   8.246    572
   3292.97   8.240    104
   3044.80   7.619     96
   3042.48   7.613    471
   3040.41   7.608    204
   3035.64   7.596    220
   3033.57   7.591    501
   3031.25   7.585    134
   2170.41   5.431   1000

in CDCl3