4-丙酰聯(lián)苯(37940-57-1)核磁圖(¹HNMR)

產(chǎn)品名稱:4-丙酰聯(lián)苯

CAS:37940-57-1

分子式:C15H14O

分子量: 210.27

InChI:InChI=1S/C15H14O/c1-2-15(16)14-10-8-13(9-11-14)12-6-4-3-5-7-12/h3-11H,2H2,1H3

InChIKey: JMBGDQSXJHLFTO-UHFFFAOYSA-N

Smiles:C(C1=CC=C(C2=CC=CC=C2)C=C1)(=O)CC

Mass

MS-IW-7218          
4'-phenylpropiophenone
C15H14O             (Mass of molecular ion:    224)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      29.0       1.1
      51.0       1.4
      63.0       1.6
      75.0       1.3
      75.5       1.5
      76.0       7.8
      76.5       3.0
      77.0       2.1
      90.5       5.0
      91.0       1.1
     126.0       1.4
     127.0       2.6
     150.0       1.5
     151.0       6.5
     152.0      27.7
     153.0      22.9
     154.0       3.6
     181.0     100.0
     182.0      14.4
     183.0       1.2
     210.0      29.2
     211.0       5.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₅ H₁₄ O	0.039 g : 0.5 ml CDCl₃
4'-phenylpropiophenone

    Assign.     Shift(ppm)

      A             8.026
      B             7.665
      C             7.612
      D             7.456
      E             7.390
      F             3.016
      G             1.243

     Hz     ppm     Int.

   3214.23   8.043     67
   3212.28   8.038    388
   3210.33   8.033    137
   3205.69   8.022    151
   3203.61   8.017    441
   3201.78   8.012     73
   3069.21   7.680     82
   3067.26   7.675    445
   3065.31   7.670    146
   3060.67   7.659    147
   3058.72   7.654    397
   3056.76   7.649     62
   3047.73   7.626    207
   3046.39   7.623    297
   3044.31   7.618     84
   3040.65   7.609    153
   3040.28   7.608    151
   3039.31   7.605    306
   3038.21   7.603    270
   3036.01   7.597     46
   2988.40   7.478    100
   2987.30   7.475    164
   2985.47   7.471     62
   2980.22   7.458    347
   2978.64   7.454    174
   2974.00   7.442    107
   2972.53   7.438    204
   2970.34   7.433     37
   2959.96   7.407     89
   2958.62   7.404    160
   2957.28   7.400     89
   2953.61   7.391     60
   2951.29   7.385    167
   2948.85   7.379     41
   2945.31   7.370     37
   2943.97   7.367     58
   2942.75   7.364     31
   1216.67   3.045    138
   1209.47   3.027    461
   1202.15   3.009    478
   1194.95   2.990    157
    504.03   1.262    492
    496.70   1.243   1000
    489.50   1.225    483

in CDCl3