二甲基-苯基二胺(3575-32-4)核磁圖(¹HNMR)

產(chǎn)品名稱:二甲基-苯基二胺

CAS:3575-32-4

分子式:C8H14Cl2N2

分子量: 209.12

InChI:InChI=1S/C8H12N2.2ClH/c1-10(2)8-5-3-4-7(9)6-8;;/h3-6H,9H2,1-2H3;2*1H

InChIKey: BZJPIQKDEGXVFG-UHFFFAOYSA-N

Smiles:C1(N(C)C)C=CC=C(N)C=1.Cl.Cl

Mass

MS-NW-6934          
N,N-dimethyl-m-phenylenediamine dihydrochloride
C8H12N2 2HCl        (Mass of molecular ion:    136)

   Source Temperature: 170 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      15.0       5.9
      17.5       1.1
      18.0       2.6
      27.0       2.3
      28.0       5.6
      30.0       1.3
      35.0       8.3
      36.0      57.7
      37.0       2.7
      38.0      17.9
      39.0       9.4
      40.0       1.5
      41.0       3.8
      42.0      11.3
      43.0       1.0
      44.0       6.7
      50.0       1.3
      51.0       2.8
      52.0       4.0
      53.0       2.9
      54.0       1.8
      59.5       2.1
      60.0       2.4
      62.0       1.1
      63.0       3.2
      64.0       2.5
      65.0      14.2
      66.0       6.9
      67.0       3.0
      67.5       3.8
      68.0       5.2
      77.0       2.6
      78.0       2.2
      79.0       1.4
      80.0       3.5
      91.0       2.0
      92.0      10.6
      93.0      27.5
      94.0       7.4
     105.0       1.7
     106.0       5.2
     107.0      10.2
     108.0       8.7
     118.0       1.6
     119.0       2.6
     120.0      11.7
     121.0      13.9
     122.0       1.6
     133.0       1.4
     135.0      63.4
     136.0     100.0
     137.0       9.0

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₈ H₁₂ N₂	0.040 g : 0.5 ml DMSO-d₆
N,N-dimethyl-m-phenylenediamine dihydrochloride

    Assign.     Shift(ppm)

      A             7.544
      B     *1      7.48
      C             7.468
      D     *1      7.224
      E             3.067

     Hz     ppm     Int.

   3024.90   7.569     24
   3016.20   7.548     60
   3008.58   7.529     49
   2992.40   7.488     44
   2984.77   7.469     87
   2891.08   7.235     41
   2883.30   7.215     38
   1225.74   3.068   1000

in DMSO-d6