2,6-二氯芐基甲基醚(33486-90-7)紅外圖譜(IR1)

產(chǎn)品名稱:2,6-二氯芐基甲基醚

CAS:33486-90-7

分子式:C8H8Cl2O

分子量: 191.05

InChI:InChI=1S/C8H8Cl2O/c1-11-5-6-7(9)3-2-4-8(6)10/h2-4H,5H2,1H3

InChIKey: QBKBHXIQLAMKOB-UHFFFAOYSA-N

Smiles:C1(Cl)=CC=CC(Cl)=C1COC

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-3475          
1,3-dichloro-2-(methoxymethyl)benzene
C8H8Cl2O            (Mass of molecular ion:    190)

   Source Temperature: 210 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       1.2
      29.0       4.7
      37.0       1.0
      38.0       1.2
      39.0       3.0
      43.0       1.1
      44.0       1.9
      45.0       8.3
      50.0       3.5
      51.0       3.3
      61.0       2.1
      62.0       4.9
      63.0       8.9
      73.0       5.4
      74.0       4.0
      75.0      10.2
      76.0       1.2
      77.0       2.5
      84.0       1.3
      85.0       1.9
      86.0       1.8
      87.0       2.3
      88.0       1.0
      89.0      15.8
      90.0       2.0
      91.0      11.1
      92.0       1.3
      97.0       2.0
      99.0       3.4
     105.0       1.3
     109.0       2.4
     110.0       1.2
     111.0      10.2
     112.0       1.8
     113.0       3.2
     123.0       9.3
     124.0       4.4
     125.0      10.0
     126.0       2.3
     127.0       2.5
     133.0       2.1
     135.0       1.3
     139.0       4.1
     141.0       1.4
     145.0       1.5
     147.0       2.0
     155.0     100.0
     156.0       9.0
     157.0      33.0
     158.0       3.0
     159.0      78.7
     160.0       6.4
     161.0      50.8
     162.0       4.1
     163.0       8.4
     173.0       2.8
     175.0       2.4
     189.0       6.0
     190.0      21.0
     191.0       5.7
     192.0      13.6
     193.0       1.8
     194.0       2.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₈ Cl₂ O	0.05 ml : 0.5 ml CDCl₃
1,3-dichloro-2-(methoxymethyl)benzene

    Assign.     Shift(ppm)

      A             7.286
      B             7.145
      C             4.704
      D             3.421

     Hz     ppm     Int.

   2916.14   7.297    307
   2910.89   7.284     31
   2907.96   7.277    440
   2862.55   7.163    200
   2855.10   7.145    173
   2854.00   7.142    163
   2846.44   7.123    122
   1880.25   4.705    675
   1367.43   3.422   1000

in CDCl3