9-芴甲醇(24324-17-2)核磁圖(¹³CNMR)

產(chǎn)品名稱(chēng):9-芴甲醇

CAS:24324-17-2

分子式:C14H12O

分子量: 196.24

InChI:InChI=1S/C14H12O/c15-9-14-12-7-3-1-5-10(12)11-6-2-4-8-13(11)14/h1-8,14-15H,9H2

InChIKey: XXSCONYSQQLHTH-UHFFFAOYSA-N

Smiles:C1(CO)C2=C(C=CC=C2)C2=C1C=CC=C2

Mass

MS-NW-7234          
9-fluorenemethanol
C14H12O             (Mass of molecular ion:    196)

   Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      31.0       1.6
      39.0       1.5
      51.0       1.1
      62.0       1.2
      63.0       3.0
      69.5       2.3
      74.0       1.3
      75.0       1.5
      76.0       1.7
      81.5       1.9
      82.0       1.7
      82.5       2.9
      86.0       1.1
      87.0       1.7
      88.0       2.1
      89.0       1.8
     115.0       3.2
     139.0       4.7
     152.0       1.5
     162.0       1.3
     163.0      11.0
     164.0       9.4
     165.0     100.0
     166.0      79.8
     167.0      11.3
     176.0       1.7
     177.0       1.4
     178.0       7.5
     179.0       1.5
     196.0      33.6
     197.0       5.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₂ O	0.036 g : 0.5 ml CDCl₃
9-fluorenemethanol

    Assign.     Shift(ppm)

      A             7.745
      B             7.566
      C             7.372
      D             7.292
      E             4.056
      F             3.967
      J             1.75

     Hz     ppm     Int.

   3099.24   7.755    842
   3091.80   7.737    921
   3027.71   7.576    757
   3026.86   7.574    755
   3020.14   7.557    861
   3019.53   7.556    856
   3013.31   7.540     30
   2954.22   7.393    392
   2946.90   7.374    859
   2939.45   7.356    539
   2935.67   7.346     58
   2921.39   7.310    642
   2920.29   7.308    655
   2913.94   7.292    933
   2912.84   7.289    917
   2906.49   7.273    388
   2905.40   7.270    367
   1628.05   4.074    159
   1621.95   4.059    368
   1615.84   4.044    292
   1588.26   3.975   1000
   1582.15   3.959    707
    700.93   1.754    362

in CDCl3