(1S,2R)-2-氨基-1,2-二苯基乙醇(23364-44-5)質(zhì)譜(MS)

產(chǎn)品名稱:(1S,2R)-2-氨基-1,2-二苯基乙醇

CAS:23364-44-5

分子式:C14H15NO

分子量: 213.28

InChI:InChI=1/C14H15NO/c15-13(11-7-3-1-4-8-11)14(16)12-9-5-2-6-10-12/h1-10,13-14,16H,15H2/t13-,14+/s3

InChIKey: GEJJWYZZKKKSEV-JJANDPSINA-N

Smiles:[C@H](C1C=CC=CC=1)(N)[C@H](C1C=CC=CC=1)O |&1:0,8,r|

Mass

MS-IW-4077          
(1S,2R)-(+)-2-amino-1,2-diphenylethanol
C14H15NO            (Mass of molecular ion:    213)

   Source Temperature: 130 °C
   Sample Temperature:  90 °C
   Direct, 75 eV

      28.0       7.1
      51.0       2.5
      77.0       9.9
      78.0       2.1
      79.0      18.7
      80.0       1.3
     104.0       2.8
     105.0       1.9
     106.0     100.0
     107.0      10.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₅ N O	0.034 g : 0.5 ml CDCl₃
(1S,2R)-(+)-2-amino-1,2-diphenylethanol

    Assign.     Shift(ppm)

      A          7.27 to 7.25
      B          7.25 to 7.23
      C          7.20 to 7.18
      D             4.691
      E             4.095
      F             2.9
      G             1.38

     Hz     ppm     Int.

   2912.60   7.288     93
   2910.77   7.284    134
   2910.03   7.282    125
   2908.94   7.279     96
   2908.20   7.277    105
   2907.35   7.275    138
   2907.10   7.275    138
   2906.49   7.273    130
   2905.52   7.271    178
   2904.17   7.267    423
   2902.34   7.263    512
   2901.12   7.260    412
   2900.27   7.258    303
   2897.71   7.251    653
   2896.85   7.249    872
   2895.39   7.245   1000
   2894.53   7.243    865
   2893.55   7.241    629
   2889.89   7.232    524
   2888.79   7.229    326
   2883.79   7.216    143
   2881.59   7.211    508
   2880.37   7.208    285
   2879.15   7.205    433
   2877.32   7.200    158
   2876.83   7.199    160
   2875.98   7.197    161
   2875.37   7.195    199
   2874.88   7.194    193
   2873.29   7.190    398
   2872.07   7.187    641
   2869.63   7.181    392
   2868.04   7.177    171
   2867.43   7.175    192
   2866.58   7.173    187
   2865.72   7.171    171
   2864.50   7.168    307
   2862.92   7.164    255
   2862.43   7.163    232
   2859.99   7.157     44
   2859.50   7.156     42
   1878.17   4.700    306
   1871.95   4.684    321
   1639.65   4.103    329
   1633.42   4.088    315

in CDCl3