N-乙基-1-萘胺(118-44-5)核磁圖(¹HNMR)

產(chǎn)品名稱:N-乙基-1-萘胺

CAS:118-44-5

分子式:C12H13N

分子量: 171.24

InChI:InChI=1S/C12H13N/c1-2-13-12-9-5-7-10-6-3-4-8-11(10)12/h3-9,13H,2H2,1H3

InChIKey: KDFFXYVOTKKBDI-UHFFFAOYSA-N

Smiles:C1(NCC)=C2C(C=CC=C2)=CC=C1

Mass

MS-NW-8561          
N-ethyl-1-naphthylamine
C12H13N             (Mass of molecular ion:    171)

   Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV

      27.0       2.2
      28.0       5.2
      29.0       1.3
      39.0       3.8
      42.0       3.1
      50.0       2.7
      51.0       5.2
      52.0       1.3
      62.0       2.5
      63.0       7.4
      64.0       2.9
      65.0       4.7
      74.0       3.0
      75.0       4.9
      76.0       2.8
      77.0      11.4
      78.0       7.3
      83.0       1.6
      85.0       1.6
      86.0       1.3
      87.0       2.2
      88.0       2.1
      89.0       5.4
     101.0       4.0
     102.0       2.1
     113.0       2.8
     114.0       3.8
     115.0      29.2
     116.0       5.1
     117.0       1.2
     126.0       7.0
     127.0      19.7
     128.0      29.8
     129.0      48.6
     130.0       5.8
     140.0       3.2
     141.0       2.2
     142.0       3.5
     143.0       3.3
     153.0       1.7
     154.0      14.8
     155.0       8.0
     156.0     100.0
     157.0      12.4
     167.0       1.7
     168.0       2.0
     169.0       1.4
     170.0       8.1
     171.0      80.1
     172.0      10.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₁₃ N	0.05 ml : 0.5 ml CDCl₃
N-ethyl-1-naphthylamine

    Assign.     Shift(ppm)

      A             7.728
      B             7.696
      C             7.38
      D             7.34
      E             7.299
      F             7.191
      G             6.534
      J             4.09
      K             3.174
      L             1.270

     Hz     ppm     Int.

   3093.63   7.741    165
   3092.29   7.738    202
   3084.47   7.718    210
   3080.32   7.708    185
   3079.59   7.706    178
   3072.14   7.688    202
   3071.41   7.686    193
   2956.42   7.398     84
   2955.08   7.395    106
   2949.58   7.381    183
   2948.36   7.378    209
   2947.27   7.375    117
   2941.89   7.362    192
   2939.45   7.356    218
   2937.62   7.351    209
   2932.50   7.338     97
   2930.91   7.334    197
   2929.57   7.331    185
   2926.03   7.322    190
   2924.32   7.318    108
   2922.73   7.314     96
   2917.97   7.302    332
   2910.28   7.283    260
   2877.56   7.201    271
   2869.38   7.180    195
   2614.99   6.544    239
   2607.42   6.525    228
   1279.42   3.202    173
   1272.34   3.184    491
   1265.14   3.166    506
   1258.06   3.148    186
    519.78   1.301     36
    514.77   1.289    565
    507.32   1.270   1000
    500.37   1.253    555

in CDCl3