2-羥基二苯甲酮(117-99-7)紅外圖譜(IR1)

產(chǎn)品名稱:2-羥基二苯甲酮

CAS:117-99-7

分子式:C13H10O2

分子量: 198.22

InChI:InChI=1S/C13H10O2/c14-12-9-5-4-8-11(12)13(15)10-6-2-1-3-7-10/h1-9,14H

InChIKey: HJIAMFHSAAEUKR-UHFFFAOYSA-N

Smiles:C(C1=CC=CC=C1O)(C1=CC=CC=C1)=O

Mass

MS-NW-6092          
2-hydroxybenzophenone
C13H10O2            (Mass of molecular ion:    198)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.2
      27.0       1.8
      28.0       1.2
      38.0       2.5
      39.0      12.9
      50.0       5.1
      51.0      14.4
      52.0       1.6
      53.0       3.6
      62.0       2.1
      63.0       5.9
      64.0       3.7
      65.0      19.3
      66.0       1.6
      70.0       1.0
      74.0       2.2
      75.0       2.4
      76.0       3.8
      77.0      40.8
      78.0       3.8
      89.0       1.0
      92.0       6.3
      93.0      11.6
      94.0       1.2
      99.0       3.3
     105.0      35.4
     106.0       3.0
     115.0       3.9
     120.0      10.6
     121.0      64.1
     122.0       5.5
     139.0       1.8
     141.0       2.5
     151.0       1.3
     152.0       2.3
     169.0       1.5
     180.0       1.1
     181.0       3.3
     197.0     100.0
     198.0      87.9
     199.0      12.1
     200.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₀ O₂	0.040 g : 0.5 ml CDCl₃
2-hydroxybenzophenone

    Assign.     Shift(ppm)

      A            12.05
      B             7.672
      C             7.59
      D             7.58
      E             7.50
      F             7.070
      G             6.868

     Hz     ppm     Int.

   4815.81  12.051   1000
   3072.80   7.689     71
   3070.97   7.685    343
   3069.69   7.681    437
   3068.22   7.678    216
   3064.74   7.669    156
   3062.73   7.664    609
   3061.26   7.660    500
   3040.38   7.608     76
   3038.92   7.604    141
   3037.63   7.601    302
   3035.98   7.597    273
   3033.79   7.592    104
   3031.77   7.587    288
   3029.57   7.581    336
   3027.93   7.577    290
   3025.54   7.571    166
   3024.08   7.567    251
   3022.80   7.564    124
   3005.95   7.522    196
   3004.48   7.518    417
   3003.93   7.517    444
   3002.47   7.513    195
   2998.99   7.505    205
   2997.70   7.501    506
   2996.24   7.498    673
   2994.59   7.494    169
   2992.94   7.489     43
   2990.74   7.484    239
   2989.09   7.480    340
   2988.18   7.477    167
   2830.29   7.082    278
   2829.19   7.080    284
   2822.05   7.062    253
   2820.95   7.059    255
   2752.99   6.889    191
   2751.89   6.886    184
   2745.85   6.871    205
   2744.93   6.869    291
   2743.83   6.866    197
   2737.79   6.851    172
   2736.69   6.848    163

in CDCl3