乙酸萘酚AS(1163-67-3)紅外圖譜(IR1)

產(chǎn)品名稱:乙酸萘酚AS

CAS:1163-67-3

分子式:C19H15NO3

分子量: 305.33

InChI:InChI=1S/C19H15NO3/c1-13(21)23-18-12-15-8-6-5-7-14(15)11-17(18)19(22)20-16-9-3-2-4-10-16/h2-12H,1H3,(H,20,22)

InChIKey: CVJGNNYDVQYHEO-UHFFFAOYSA-N

Smiles:C1=C2C(C=CC=C2)=CC(OC(C)=O)=C1C(NC1=CC=CC=C1)=O

Mass

MS-NW-2313          
3-phenylcarbamoyl-2-naphthyl acetate
C19H15NO3           (Mass of molecular ion:    305)

   Source Temperature: 240 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      14.0       1.8
      15.0       1.7
      17.0       1.0
      18.0       4.9
      28.0       1.8
      39.0       3.7
      42.0       3.8
      43.0      11.3
      51.0       2.5
      62.0       1.5
      63.0       4.1
      64.0       1.6
      65.0       4.3
      66.0       1.2
      75.0       1.1
      77.0       4.0
      87.0       1.2
      88.0       3.0
      89.0       2.8
      93.0      23.9
      94.0       1.7
     113.0       4.7
     114.0      17.0
     115.0      37.5
     116.0       3.7
     117.0       1.3
     118.0       1.0
     140.0       1.0
     142.0      26.7
     143.0       4.9
     169.0       1.7
     170.0     100.0
     171.0      95.5
     172.0      11.2
     173.0       1.0
     213.0       4.6
     217.0       1.6
     245.0       6.6
     246.0       1.6
     262.0       2.9
     263.0      86.3
     264.0      16.0
     265.0       1.8
     305.0       5.0
     306.0       1.1

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₉ H₁₅ N O₃	0.040 g : 0.5 ml DMSO-d₆
3-phenylcarbamoyl-2-naphthyl acetate

    Assign.     Shift(ppm)

      A            10.5
      B             8.333
      C             8.091
      D             7.980
      E             7.784
      F             7.77
      G     *1      7.65
      J     *1      7.61
      K             7.372
      L             7.120
      M             2.254

     Hz     ppm     Int.

   4215.94  10.550    135
   3330.52   8.334    210
   3238.02   8.103     71
   3230.14   8.083     78
   3193.32   7.991     77
   3185.45   7.971     85
   3111.27   7.785    359
   3102.47   7.763    141
   3064.19   7.668     33
   3062.73   7.664     41
   3057.23   7.650     80
   3055.95   7.647     78
   3054.85   7.644     45
   3049.54   7.631     88
   3047.89   7.627    136
   3046.24   7.623     91
   3040.93   7.609     43
   3039.83   7.607     74
   3038.55   7.604     79
   3033.05   7.590     37
   3031.59   7.586     33
   2954.11   7.392    113
   2952.28   7.388     51
   2949.90   7.382     30
   2946.60   7.373    171
   2942.57   7.363     42
   2940.01   7.357     49
   2938.36   7.353    122
   2853.37   7.140     37
   2852.27   7.137     68
   2851.35   7.135     47
   2844.94   7.119    110
   2838.71   7.103     30
   2837.62   7.101     50
   2836.52   7.098     31
    901.00   2.255   1000

in DMSO-d6