二苯基硒醚(1132-39-4)質(zhì)譜(MS)

產(chǎn)品名稱:二苯基硒醚

CAS:1132-39-4

分子式:C12H10Se

分子量: 233.17

InChI:InChI=1S/C12H10Se/c1-3-7-11(8-4-1)13-12-9-5-2-6-10-12/h1-10H

InChIKey: ORQWTLCYLDRDHK-UHFFFAOYSA-N

Smiles:[Se](C1=CC=CC=C1)C1=CC=CC=C1

Mass

MS-NW-7219          
diphenyl diselenide
C12H10Se2           (Mass of molecular ion:    314)

   Source Temperature: 220 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.4
      27.0       3.0
      28.0      13.1
      32.0       3.5
      37.0       1.4
      38.0       2.0
      39.0      15.7
      50.0      17.9
      51.0      43.2
      52.0       3.4
      62.0       1.3
      63.0       4.5
      65.0      13.9
      66.0       1.6
      73.0       1.0
      74.0       6.4
      75.0       6.9
      76.0       9.2
      77.0      89.4
      78.0      20.6
      79.0       1.4
      80.0       1.7
      91.0       1.6
      93.0       3.1
     103.0       1.8
     104.0       1.2
     105.0       3.1
     106.0       1.6
     107.0       2.2
     110.0       1.7
     113.0       2.2
     114.0       1.9
     115.0       5.6
     116.0       1.5
     117.0      10.8
     118.0       1.2
     119.0       2.2
     127.0       1.5
     128.0       1.8
     129.0       2.8
     130.0       2.5
     131.0       2.7
     151.0       2.5
     152.0       5.9
     153.0      20.0
     154.0      56.9
     155.0      49.6
     156.0      11.3
     157.0     100.0
     158.0      13.2
     159.0      18.3
     160.0       2.4
     186.0       1.2
     228.0       1.2
     229.0       1.8
     230.0       8.6
     231.0       8.9
     232.0      19.2
     233.0       8.7
     234.0      33.1
     235.0       6.4
     236.0       7.0
     237.0       4.1
     238.0       1.1
     239.0       1.1
     306.0       3.2
     307.0       3.7
     308.0      13.7
     309.0      10.2
     310.0      34.4
     311.0      22.2
     312.0      57.4
     313.0      11.0
     314.0      64.2
     315.0       8.6
     316.0      19.7
     317.0       2.8
     318.0       2.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₂ H₁₀ Se₂	0.038 g : 0.5 ml CDCl₃
diphenyl diselenide

    Assign.     Shift(ppm)

      A             7.592
      B          7.33 to 7.150

     Hz     ppm     Int.

    689.19   7.696     47
    686.94   7.671    134
    685.75   7.657    361
    684.44   7.643    219
    683.56   7.633    224
    682.06   7.616    483
    680.69   7.601    377
    678.63   7.578    528
    677.56   7.566    341
    676.13   7.550    599
    673.63   7.522    130
    672.19   7.506     97
    671.13   7.494     59
    670.50   7.487     51
    661.31   7.384     46
    655.94   7.325     93
    655.38   7.318    134
    655.00   7.314    136
    653.88   7.302    278
    653.06   7.292    233
    652.56   7.287    265
    651.25   7.272    743
    650.63   7.265    600
    650.13   7.260    461
    649.13   7.248    443
    647.56   7.231    818
    646.38   7.218    422
    645.81   7.211    309
    644.75   7.200   1000
    643.63   7.187    256
    641.06   7.158     89

in CDCl3