1-氨基-2-甲基萘鹽酸鹽(111180-78-0)核磁圖(¹HNMR)

產(chǎn)品名稱:1-氨基-2-甲基萘鹽酸鹽

CAS:111180-78-0

分子式:C11H12ClN

分子量:

InChI:InChI=1S/C11H11N.ClH/c1-8-6-7-9-4-2-3-5-10(9)11(8)12;/h2-7H,12H2,1H3;1H

InChIKey: PEBKGVSIRFSIGW-UHFFFAOYSA-N

Smiles:C12C=CC=CC1=CC=C(C)C=2N.Cl

Mass

MS-IW-7345          
2-methyl-1-naphthylamine hydrochloride
C11H11N HCl         (Mass of molecular ion:    157)

   Source Temperature: 150 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      36.0       8.9
      38.0       3.0
      51.0       1.6
      63.0       1.8
      64.0       2.1
      64.5       1.1
      65.0       3.7
      65.5       4.3
      76.5       1.5
      77.0       4.5
      77.5       3.8
      78.0       5.4
      78.5       8.8
      79.0       1.1
     115.0       2.3
     116.0       1.7
     126.0       1.0
     127.0       5.9
     128.0      10.6
     129.0      12.4
     130.0       2.7
     139.0       3.6
     140.0       4.2
     141.0       3.5
     154.0       2.6
     156.0      61.6
     157.0     100.0
     158.0      12.0

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₁ H₁₁ N	0.040 g : 0.5 ml DMSO-d₆
2-methyl-1-naphthylamine hydrochloride

    Assign.     Shift(ppm)

      A             8.364
      B             7.968
      C     *1      7.846
      D             7.632
      E             7.556
      F     *1      7.434
      G             2.295

     Hz     ppm     Int.

   3348.65   8.379    121
   3340.59   8.359    127
   3340.04   8.358    128
   3188.75   7.979    117
   3181.05   7.960    128
   3138.74   7.854    150
   3130.32   7.833    167
   3059.43   7.656     58
   3057.96   7.652     64
   3052.47   7.638     98
   3051.00   7.635    124
   3049.54   7.631     69
   3044.04   7.617     91
   3042.58   7.614     84
   3027.19   7.575     93
   3026.28   7.573     99
   3019.13   7.555    131
   3018.22   7.553    101
   3012.17   7.538     62
   3011.26   7.535     59
   2975.36   7.445    206
   2966.75   7.424    187
   1037.46   2.596   1000

in DMSO-d6