環(huán)己基丙酸乙酯(10094-36-7)質(zhì)譜(MS)

產(chǎn)品名稱:環(huán)己基丙酸乙酯

CAS:10094-36-7

分子式:C11H20O2

分子量: 184.28

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-7611          
ethyl cyclohexanepropionate
C11H20O2            (Mass of molecular ion:    184)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.1
      18.0       2.1
      26.0       2.1
      27.0      15.8
      28.0       5.7
      29.0      23.4
      30.0       1.1
      31.0       3.6
      39.0      12.5
      40.0       2.4
      41.0      38.8
      42.0       5.1
      43.0       5.7
      45.0      13.4
      51.0       1.5
      52.0       1.0
      53.0       6.6
      54.0       9.6
      55.0      63.3
      56.0       5.0
      57.0       5.0
      60.0      25.8
      61.0      25.0
      62.0       1.0
      65.0       1.7
      66.0       1.4
      67.0      19.0
      68.0       6.5
      69.0      13.7
      70.0      17.9
      71.0       3.0
      73.0      36.5
      74.0      14.6
      75.0       4.5
      77.0       2.0
      78.0       1.0
      79.0       6.3
      80.0       2.0
      81.0      14.4
      82.0       4.6
      83.0      15.9
      84.0       2.0
      88.0      81.8
      89.0      19.4
      90.0       1.2
      91.0       2.4
      92.0       1.0
      93.0       4.6
      94.0      10.2
      95.0      16.3
      96.0      18.0
      97.0      46.8
      98.0       4.1
     101.0     100.0
     102.0      10.7
     103.0       1.2
     109.0       3.9
     110.0       2.9
     111.0       1.0
     119.0       1.3
     120.0       2.3
     121.0      20.7
     122.0       2.4
     127.0       3.0
     137.0       1.5
     138.0       6.8
     139.0      15.7
     140.0       1.7
     155.0      11.8
     156.0       1.6
     184.0       1.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₂₀ O₂	0.05 ml : 0.5 ml CDCl₃
ethyl cyclohexanepropionate

    Assign.     Shift(ppm)

      A             4.119
      B             2.297
      C             1.697
      D             1.64
      E             1.522
      F             1.250
      G             1.20
      J             0.90

     Hz     ppm     Int.

   1657.23   4.147    171
   1650.15   4.129    467
   1642.94   4.111    480
   1635.86   4.094    175
    926.27   2.318    265
    920.78   2.304     64
    918.46   2.299    298
    917.36   2.296    173
    915.53   2.291     76
    910.52   2.279    290
    619.87   1.552    133
    612.92   1.534    197
    611.94   1.532    162
    609.38   1.525     52
    608.15   1.522     49
    606.20   1.517     96
    604.25   1.512    201
    597.29   1.495    133
    514.16   1.287     30
    507.20   1.270    563
    500.00   1.252   1000
    492.80   1.234    624
    488.89   1.224     94
    484.01   1.212    127
    480.83   1.204    147
    471.07   1.179    121
    468.99   1.174    145
    462.52   1.158     48
    460.08   1.152     73
    457.40   1.145     45
    448.00   1.121     46
    375.49   0.940     48
    372.68   0.933     56
    363.40   0.910     89
    360.96   0.904    113
    350.22   0.877     85
    339.97   0.851     30

in CDCl3