Diethyl azodicarboxylate(1972-28-7) 13C NMR
Product NameDiethyl azodicarboxylate
CAS1972-28-7
Molecular FormulaC6H10N2O4
Molecular Weight174.15
InChIInChI=1S/C6H10N2O4/c1-3-11-5(9)7-8-6(10)12-4-2/h3-4H2,1-2H3
InChIKey FAMRKDQNMBBFBR-UHFFFAOYSA-N
SmilesN(C(OCC)=O)=NC(OCC)=O
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MassMS-NW-1286 diethyl azodiformate C6H10N2O4 (Mass of molecular ion: 174)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.2 26.0 1.1 27.0 15.0 28.0 20.4 29.0 100.0 30.0 2.2 31.0 2.2 32.0 4.4 43.0 1.6 44.0 1.1 45.0 2.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H10 N2 O4 0.04 ml : 0.5 ml CDCl3 diethyl azodiformate 
Assign. Shift(ppm)
A 4.505 B 1.444
Hz ppm Int.414.56 4.629 125 407.25 4.548 427 400.13 4.468 445 393.13 4.390 145 136.25 1.522 465 129.19 1.443 1000 122.00 1.363 414
in CDCl3
CCl4 solution
liquid film
