Company Name:
Shanghai Daken Advanced Materials Co.,Ltd
Tel:
+86-371-66670886
Email:
info@dakenam.com
Products Intro:
Product Name:2,4-diphenyl-6-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1,3,5-triazine CAS:1269508-31-7 Purity:99% Package:1KG,5KG,100KG
Related articles 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine: Uses, Synthesis and Application 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine is an OLED intermediate. Dec 14,2022
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Basic information
Product Name: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Synonyms: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine ;2-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-4,6-diphenyl-1,3,5-triazine ;1,3,5-Triazine, 2,4-diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]- ;3-(4,6-Diphenyl-1,3,5-triazine-2-yl)phenylboronic Acid Pinacol Ester ;2-[3-(4,6-Diphenyl-1,3,5-triazin-2-yl)phenyl]-4,4,5,5-tetramethyl-1,3,2-dioxaborolane ;2-dioxaborolan-2-yl)phenyl]-1 ;4-Diphenyl-6-[3-(4 ;2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-... CAS: 1269508-31-7 MF: C27H26BN3O2 MW: 435.33 EINECS: Product Categories: OLED Mol File: 1269508-31-7.mol
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Chemical Properties
Melting point 204 °C Boiling point 641.3±57.0 °C(Predicted) density 1.21±0.1 g/cm3(Predicted) pka 0.92±0.10(Predicted) form powder to crystal color White to Almost white InChI InChI=1S/C27H26BN3O2/c1-26(2)27(3,4)33-28(32-26)22-17-11-16-21(18-22)25-30-23(19-12-7-5-8-13-19)29-24(31-25)20-14-9-6-10-15-20/h5-18H,1-4H3 InChIKey FXHGBACNYDFALU-UHFFFAOYSA-N SMILES N1=C(C2=CC=CC(B3OC(C)(C)C(C)(C)O3)=C2)N=C(C2=CC=CC=C2)N=C1C1=CC=CC=C1
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Usage And Synthesis
Uses 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine can be used as an intermediate in organic
synthesis, mainly used in laboratory research and development and
chemical production processes. Synthesis
15.0 g of 2-(3-Bromophenyl)-4,6-diphenyl-l,3,5-
triazine (32.4 mmol), 12.3 g of bis(pinacolato)diboron (48.6
mmol), 529 mg of Pd(dppf)Cl2.CH2Cl2 (0.647 mmol), 9.53
g of potassium acetate (97.1 mmol) and 323 ml of dioxane
were put into a 1-neck round flask and reacted under reflux
at 90° C. for 12 hours. After completion of the reaction, the solvent was removed under reduced pressure. The produced
solid was dissolved in dichloromethane and then filtered
through a Celite filter and washed with dichloromethane.
The solvent was removed under reduced pressure and the
resultant compound was crystallized with methanol to obtain
16.0 g of solid compound (2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine) (yield: 96.8%).
2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine Preparation Products And Raw materials