- Minocycline Impurity
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- $0.00 / 100mg
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2025-05-21
- CAS:2449-05-0
- Min. Order: 10mg
- Purity: 98
- Supply Ability: 100000
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| | Dibenzyl azodicarboxylate Basic information |
| | Dibenzyl azodicarboxylate Chemical Properties |
| Melting point | 43-47 °C (lit.) | | Boiling point | 439.72°C (rough estimate) | | density | 1.2028 (rough estimate) | | refractive index | 1.6240 (estimate) | | Fp | >230 °F | | storage temp. | 2-8°C | | form | Crystalline Powder | | color | Yellow to orange | | Sensitive | Light Sensitive | | BRN | 2298734 | | InChI | InChI=1S/C16H14N2O4/c19-15(21-11-13-7-3-1-4-8-13)17-18-16(20)22-12-14-9-5-2-6-10-14/h1-10H,11-12H2 | | InChIKey | IRJKSAIGIYODAN-ISLYRVAYSA-N | | SMILES | N(C(OCC1=CC=CC=C1)=O)=NC(OCC1=CC=CC=C1)=O | | CAS DataBase Reference | 2449-05-0(CAS DataBase Reference) | | EPA Substance Registry System | Diazenedicarboxylic acid, bis(phenylmethyl) ester (2449-05-0) |
| | Dibenzyl azodicarboxylate Usage And Synthesis |
| Chemical Properties | yellow to orange crystalline powder | | Uses | Dibenzyl azodicarboxylate was used as electrophilic reagent in the synthesis of C-glycosyl α-amino acids via proline-catalyzed α-amination of C-glycosylalkyl aldehydes. It was used in enantioselective synthesis of optically active pyrazolidine derivatives. | | Uses | Dibenzyl azodicarboxylate is a reagent used in the synthesis of Minocycline-d6 (M344797). Minocycline-d6 is a labeled second generation tetracycline antibiotic. Antibacterial. | | General Description | Dibenzyl azodicarboxylate undergoes[4+2] cycloaddition reaction with glycal to yield 2-aminoglycosides. | | Synthesis | PIDA (phenyliodine diacetate) and DCM (dichloromethane) were added to compound dibenzyl hydrazine-1,2-dicarboxylate, and the mixture was reacted with stirring at room temperature for 30 minutes to obtain DBAD (dibenzyl azodicarboxylate) in a yield of 97%. |
| | Dibenzyl azodicarboxylate Preparation Products And Raw materials |
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