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2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole

2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole ??? ???
?? ??:
1257220-44-2
???:
2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole
???(??):
BPCF;2-Bromo-7,7-dimethyl-5-phenyl-indeno[2,1-b]carbazole;2-bromo-7,7-dimethyl-5-phenyl-5,7-dihydroindeno[2,1-b]carbaz...;2-bromo-7,7-dimethyl-5-phenyl-5,7-dihydroindeno[2,1-b]carbazole;2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole;Indeno[2,1-b]carbazole, 2-bromo-5,7-dihydro-7,7-dimethyl-5-phenyl-;7-bromo-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole;6-bromo-11,11-dimethyl-9-phenyl-5,9,10,11-tetrahydroindeno[2,1-b]carbaz;6-bromo-11,11-dimethyl-9-phenyl-5,9,10,11-tetrahydroindeno[2,1-b]carbazole;7-Bromo-12,12-dimethyl-10-phenyl-10,12-dihydro-10-aza-indeno[2,1-b]fluorene
CBNumber:
CB72686645
???:
C27H20BrN
??? ??:
438.36
MOL ??:
1257220-44-2.mol

2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole ??

?? ?
584.2±32.0 °C(Predicted)
??
1.35±0.1 g/cm3(Predicted)

??

2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole C??? ??, ??, ??

??

2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical industry during production process.

Synthesis

Synthesis_1257220-44-2
The resulting 12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole (7.5 g) and DMF (53 ml) were added to a reaction vessel. N-bromosuccinimide (3.72 g) was added under ice-cooled conditions, and the mixture was stirred for 9 hours and then left for one night. Water (260 ml) was added, and the mixture was subjected to filtration to obtain a brownish white powder of 7-bromo-12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole (8.67 g; yield 94.6%).

2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole ?? ?? ? ???

???

2-Amino-9,9-dimethylfluorene 9-??-9H-????-3-???? 5,7-????-7,7-???-5-??-???[2,1-b]???? 5,7-????-7,7-???-???[2,1-b]???? N-????????? ?????? 1-Bromo-2-iodobenzene ??2-????????

?? ??

2-BroMo-5,7-dihydro-7,7-diMethyl-5-phenyl-indeno[2,1-b]carbazole ?? ??

???( 48)?? ??
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