1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene
- CAS No.
- 41481-63-4
- Chemical Name:
- 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene
- Synonyms
- Diallyl Ether Bisphenol-S;BIS(4-ALLYLOXYPHENYL)SULFONE;Bis(p-allyloxyphenyl) sulfone;4,4'-Sulfonylbis((allyloxy)benzene);Bis-[4-(2propenyloxy)-phenyl]-sulfone;1-(benzenesulfonyl)-4-prop-2-enoxybenzene;Sulfonylbis(4,1-phenylene)bis(allyl ether);1,1'-PHENYLSULFONYL-4,4'-DIENEPROPYL ETHER;1,1'-sulfonylbis[4-(2-propenyl)oxy-benzene];1,1'-Phenylsulfonyl-4,4'-Dienepropyl(2)Ether
- CBNumber:
- CB0696083
- Molecular Formula:
- C18H18O4S
- Molecular Weight:
- 330.4
- MDL Number:
- MFCD00506306
- MOL File:
- 41481-63-4.mol
Melting point | 141-142 °C(Solv: ethanol (64-17-5)) |
---|---|
Boiling point | 500.7±45.0 °C(Predicted) |
Density | 1.171±0.06 g/cm3(Predicted) |
storage temp. | -20°C Freezer, Under inert atmosphere |
solubility | DMSO (Slightly), Methanol (Slightly) |
form | Solid |
color | White to Off-White |
CAS DataBase Reference | 41481-63-4(CAS DataBase Reference) |
1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene price
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
TRC | A614508 | bis(4-Allyloxyphenyl)sulfone | 41481-63-4 | 10g | $245 | 2021-12-16 | Buy |
Biosynth Carbosynth | FB147064 | Bis(4-allyloxyphenyl)sulfone | 41481-63-4 | 100g | $376 | 2021-12-16 | Buy |
AK Scientific | P143 | 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene] | 41481-63-4 | 100g | $557 | 2021-12-16 | Buy |
Biosynth Carbosynth | FB147064 | Bis(4-allyloxyphenyl)sulfone | 41481-63-4 | 250g | $752.5 | 2021-12-16 | Buy |
AK Scientific | P143 | 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene] | 41481-63-4 | 250g | $1065 | 2021-12-16 | Buy |
1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Chemical Properties,Uses,Production
Uses
1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is a useful research chemical.
Chemical Properties
White crystalline powder
Preparation
The preparation of 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is as follows:2400g water, 216g caustic soda lye of 48% strength, 600g 4,4'-dihydroxydiphenyl sulfone and 204g Allyl chloride were mixed and the reaction was carried out at 55-60°C and autogenously generated pressure of 0.8-1. Okg/cm2 for 8 hours. 204g caustic soda lye of 48% strength was added in the reaction mixture, and maintained for 1 hour at 80°C thereafter filtered at 80°C to remove 4,4'-diallyloxydiphenyl sulfone. Further, the filtrate solution was treated with 5g activated carbon and 5g sequestering agent at 85- 90°C. The pH of filtrated solution was adjusted to 8.9 with 20% sulfuric acid and cooled to 35°C. The precipitate was separated by filtration and slurred in water. The pH was adjusted to 4.94 with 20% sulfuric acid and the precipitate was separated by filtration, and washed with water and dried to obtain 615g the product 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity. The yield was 93.5% with respect to 4,4'-dihydroxydiphenyl sulfone. The wet cake of 4,4'-diallyloxydiphenyl sulfone was slurred in 100g of 5%w/v aqueous solution of sodium hydroxide and refluxed for 1 hour, then cooled to 80°C. The precipitate was filtered, washed with water and dried to obtain 45g of 4,4'-diallyloxy diphenyl sulfone of 91.9% purity. The yield was 6% with respect to 4,4'-dihydroxydiphenyl sulfone. pH of the mother liquor obtained after separation of 4-allyloxy 4'-hydroxydiphenyl sulfone, was adjusted to 4.5 with 20% sulfuric acid. The precipitate was separated by filtration, washed with water and dried to obtain 33g of 4,4'-dihydroxydiphenyl sulfone of 87.9% purity. The conversion of 4,4'-dihydroxydiphenyl sulfone was 94.50%.; 595g of 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity was dissolved in 230g of 48% strength caustic soda lye and 1000g water, treated with 5g activated carbon and 5g sequestering agent at 85-90°C. The slurry was filtered and pH of the filtrate was adjusted to 8.95 with 20% sulfuric acid and then cooled to 35°C. The precipitate was separated by filtration, slurried in water and the pH was adjusted to 5.0 with 20% sulfuric acid. The slurry was filtrated and the precipitate was washed with water and dried to obtain 563g of 4- allyloxy 4'-hydroxydiphenyl sulfone of 99.273% purity.
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1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | |
---|---|---|---|---|---|
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | info@dakenam.com | China | 18949 | 58 |
ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32965 | 60 |
career henan chemical co | +86-0371-86658258 +8613203830695 | sales@coreychem.com | China | 29871 | 58 |
Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10311 | 58 |
Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | sales@chemdad.com | China | 39894 | 58 |
SIMAGCHEM CORP | +86-13806087780 | sale@simagchem.com | China | 17365 | 58 |
Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
Dayang Chem (Hangzhou) Co.,Ltd. | 571-88938639 +8617705817739 | info@dycnchem.com | China | 52849 | 58 |
Henan Alfa Chemical Co., Ltd | China | 12003 | 58 | ||
Hangzhou MolCore BioPharmatech Co.,Ltd. | +86-057181025280; +8617767106207 | sales@molcore.com | China | 49734 | 58 |
View Lastest Price from 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene manufacturers
Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
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2022-09-20 | 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
|
US $0.00-0.00 / kg | 1kg | 98% | 1Ton | Henan Aochuang Chemical Co.,Ltd. | |
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2021-08-12 | 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
|
US $15.00-10.00 / KG | 1KG | 99%+ HPLC | Monthly supply of 1 ton | Zhuozhou Wenxi import and Export Co., Ltd | |
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2019-07-06 | 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
|
US $2.00 / kg | 1kg | 99% | ask | Career Henan Chemical Co |
-
- 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
- US $0.00-0.00 / kg
- 98%
- Henan Aochuang Chemical Co.,Ltd.
-
- 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
- US $15.00-10.00 / KG
- 99%+ HPLC
- Zhuozhou Wenxi import and Export Co., Ltd
-
- 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
- US $2.00 / kg
- 99%
- Career Henan Chemical Co