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ChemicalBook >> CAS DataBase List >>1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene

CAS No.
41481-63-4
Chemical Name:
1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene
Synonyms
Diallyl Ether Bisphenol-S;BIS(4-ALLYLOXYPHENYL)SULFONE;Bis(p-allyloxyphenyl) sulfone;4,4'-Sulfonylbis((allyloxy)benzene);Bis-[4-(2propenyloxy)-phenyl]-sulfone;1-(benzenesulfonyl)-4-prop-2-enoxybenzene;Sulfonylbis(4,1-phenylene)bis(allyl ether);1,1'-PHENYLSULFONYL-4,4'-DIENEPROPYL ETHER;1,1'-sulfonylbis[4-(2-propenyl)oxy-benzene];1,1'-Phenylsulfonyl-4,4'-Dienepropyl(2)Ether
CBNumber:
CB0696083
Molecular Formula:
C18H18O4S
Molecular Weight:
330.4
MDL Number:
MFCD00506306
MOL File:
41481-63-4.mol
Last updated:2024-06-05 20:42:10

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Properties

Melting point 141-142 °C(Solv: ethanol (64-17-5))
Boiling point 500.7±45.0 °C(Predicted)
Density 1.171±0.06 g/cm3(Predicted)
storage temp. -20°C Freezer, Under inert atmosphere
solubility DMSO (Slightly), Methanol (Slightly)
form Solid
color White to Off-White
CAS DataBase Reference 41481-63-4(CAS DataBase Reference)

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene price

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC A614508 bis(4-Allyloxyphenyl)sulfone 41481-63-4 10g $245 2021-12-16 Buy
Biosynth Carbosynth FB147064 Bis(4-allyloxyphenyl)sulfone 41481-63-4 100g $376 2021-12-16 Buy
AK Scientific P143 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene] 41481-63-4 100g $557 2021-12-16 Buy
Biosynth Carbosynth FB147064 Bis(4-allyloxyphenyl)sulfone 41481-63-4 250g $752.5 2021-12-16 Buy
AK Scientific P143 1,1'-Sulfonylbis[4-(2-propenyl)oxy-benzene] 41481-63-4 250g $1065 2021-12-16 Buy
Product number Packaging Price Buy
A614508 10g $245 Buy
FB147064 100g $376 Buy
P143 100g $557 Buy
FB147064 250g $752.5 Buy
P143 250g $1065 Buy

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Chemical Properties,Uses,Production

Uses

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is a useful research chemical.

Chemical Properties

White crystalline powder

Preparation

The preparation of 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene is as follows:2400g water, 216g caustic soda lye of 48% strength, 600g 4,4'-dihydroxydiphenyl sulfone and 204g Allyl chloride were mixed and the reaction was carried out at 55-60°C and autogenously generated pressure of 0.8-1. Okg/cm2 for 8 hours. 204g caustic soda lye of 48% strength was added in the reaction mixture, and maintained for 1 hour at 80°C thereafter filtered at 80°C to remove 4,4'-diallyloxydiphenyl sulfone. Further, the filtrate solution was treated with 5g activated carbon and 5g sequestering agent at 85- 90°C. The pH of filtrated solution was adjusted to 8.9 with 20% sulfuric acid and cooled to 35°C. The precipitate was separated by filtration and slurred in water. The pH was adjusted to 4.94 with 20% sulfuric acid and the precipitate was separated by filtration, and washed with water and dried to obtain 615g the product 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity. The yield was 93.5% with respect to 4,4'-dihydroxydiphenyl sulfone. The wet cake of 4,4'-diallyloxydiphenyl sulfone was slurred in 100g of 5%w/v aqueous solution of sodium hydroxide and refluxed for 1 hour, then cooled to 80°C. The precipitate was filtered, washed with water and dried to obtain 45g of 4,4'-diallyloxy diphenyl sulfone of 91.9% purity. The yield was 6% with respect to 4,4'-dihydroxydiphenyl sulfone. pH of the mother liquor obtained after separation of 4-allyloxy 4'-hydroxydiphenyl sulfone, was adjusted to 4.5 with 20% sulfuric acid. The precipitate was separated by filtration, washed with water and dried to obtain 33g of 4,4'-dihydroxydiphenyl sulfone of 87.9% purity. The conversion of 4,4'-dihydroxydiphenyl sulfone was 94.50%.; 595g of 4-allyloxy 4'-hydroxydiphenyl sulfone of 96% purity was dissolved in 230g of 48% strength caustic soda lye and 1000g water, treated with 5g activated carbon and 5g sequestering agent at 85-90°C. The slurry was filtered and pH of the filtrate was adjusted to 8.95 with 20% sulfuric acid and then cooled to 35°C. The precipitate was separated by filtration, slurried in water and the pH was adjusted to 5.0 with 20% sulfuric acid. The slurry was filtrated and the precipitate was washed with water and dried to obtain 563g of 4- allyloxy 4'-hydroxydiphenyl sulfone of 99.273% purity.

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80-09-1
106-95-6
41481-63-4
Synthesis of 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene from Bis(4-hydroxyphenyl) Sulfone and Allyl bromide

1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene Preparation Products And Raw materials

Global( 95)Suppliers
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Shanghai Daken Advanced Materials Co.,Ltd
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ATK CHEMICAL COMPANY LIMITED
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Shenzhen Nexconn Pharmatechs Ltd
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SIMAGCHEM CORP
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Dayang Chem (Hangzhou) Co.,Ltd.
571-88938639 +8617705817739 info@dycnchem.com China 52849 58
Henan Alfa Chemical Co., Ltd
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Hangzhou MolCore BioPharmatech Co.,Ltd.
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View Lastest Price from 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene pictures 2022-09-20 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
US $0.00-0.00 / kg 1kg 98% 1Ton Henan Aochuang Chemical Co.,Ltd.
1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene pictures 2021-08-12 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
US $15.00-10.00 / KG 1KG 99%+ HPLC Monthly supply of 1 ton Zhuozhou Wenxi import and Export Co., Ltd
1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene pictures 2019-07-06 1-Prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene
41481-63-4
US $2.00 / kg 1kg 99% ask Career Henan Chemical Co
1,1'-sulfonylbis[4-(2-propenyl)oxy-benzene] 1,1'-PHENYLSULFONYL-4,4'-DIENEPROPYL ETHER 1,1'-Phenylsulfonyl-4,4'-Dienepropyl(2)Ether Bis-[4-(2propenyloxy)-phenyl]-sulfone Bis(p-allyloxyphenyl) sulfone Sulfonylbis(4,1-phenylene)bis(allyl ether) 1-allyloxy-4-(4-allyloxyphenyl)sulfonyl-benzene 1-prop-2-enoxy-4-(4-prop-2-enoxyphenyl)sulfonyl-benzene BIS(4-ALLYLOXYPHENYL)SULFONE 1-(benzenesulfonyl)-4-prop-2-enoxybenzene Diallyl Ether Bisphenol-S Benzene, 1,1'-sulfonylbis[4-(2-propen-1-yloxy)- 4,4'-Sulfonylbis((allyloxy)benzene) 1,1'-Sulfonylbis[4-(prop-2-en-1-yloxy)benzene 41481-63-4 C18H18O4S Industrial/Fine Chemicals Aromatics
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