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Allyl triflate

Allyl triflate Struktur
41029-45-2
CAS-Nr.
41029-45-2
Englisch Name:
Allyl triflate
Synonyma:
Allyl triflate;Allyl Trifluoromethanesulfonate;Methanesulfonic acid, 1,1,1-trifluoro-, 2-propen-1-yl ester
CBNumber:
CB12488306
Summenformel:
C4H5F3O3S
Molgewicht:
190.14
MOL-Datei:
41029-45-2.mol

Allyl triflate Eigenschaften

Siedepunkt:
16.6°C
Dichte
1.456 (estimate)
L?slichkeit
sol chlorinated hydrocarbons.
Farbe
colorless liquid.

Sicherheit

Allyl triflate Chemische Eigenschaften,Einsatz,Produktion Methoden

Synthesis Reference(s)

The Journal of Organic Chemistry, 42, p. 3109, 1977 DOI: 10.1021/jo00439a001

Synthese

Allyl triflate is prepared by the reaction of Trifluoromethanesulfonic Anhydride (1 equiv) and allyl alcohol (1 equiv) in the presence of pyridine (1 equiv) in carbon tetrachloride at 0 °C.1 The insoluble pyridine salt is removed by filtration through sodium sulfate, and the resulting solution is used directly for allylation reactions. The yield of the reaction is reported to be 75 ± 5% based on quantitative NMR analysis of aliquots.

Allyl triflate Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Allyl triflate Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

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  • Allyl triflate
  • Allyl Trifluoromethanesulfonate
  • Methanesulfonic acid, 1,1,1-trifluoro-, 2-propen-1-yl ester
  • 41029-45-2
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