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ChemicalBook--->CAS DataBase List--->68696-18-4

68696-18-4

68696-18-4 Structure

68696-18-4 Structure
IdentificationMore
[Name]

TETRAETHYLAMMONIUM CHLORIDE MONOHYDRATE
[CAS]

68696-18-4
[Synonyms]

TEA CHLORIDE HYDRATE
TETRAETHYLAMMONIUM CHLORIDE HYDRATE
TETRAETHYLAMMONIUM CHLORIDE MONOHYDRATE
Tetramethylammonium chloride hydrate
Tetraethylammonium chloride monohydrate, 98+%
[EINECS(EC#)]

200-267-5
[Molecular Formula]

C8H22ClNO
[MDL Number]

MFCD00149992
[Molecular Weight]

183.72
[MOL File]

68696-18-4.mol
Chemical PropertiesBack Directory
[Melting point ]

ca 110℃
[density ]

1.0801
[storage temp. ]

Store below +30°C.
[solubility ]

1410g/l
[form ]

Crystalline
[PH]

6.5 (100g/l, H2O, 20℃)
[Water Solubility ]

Soluble in water.
[Sensitive ]

Hygroscopic
[Merck ]

14,9200
[BRN ]

3563247
[CAS DataBase Reference]

68696-18-4(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xn
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[RTECS ]

BS6125000
[F ]

3-10
[TSCA ]

Yes
[HS Code ]

2923 90 00
Hazard InformationBack Directory
[Uses]

Phase transfer catalystTetraethylammonium chloride monohydrate is used in the preparation of 2,3,4,6-tetra-O-acetyl-beta-D-glucopyranosyl chloride by reacting with 1,2-O-acetoxonium-3,4,6-tri-O-acetyl-alfaD-glucopyranose perchlorate.
[Purification Methods]

Crystallise the chloride from EtOH by adding diethyl ether, from warm water by adding EtOH and diethyl ether, from dimethylacetamide or from CH2Cl2 by addition of diethyl ether. Dry it over P2O5 in vacuum for several days. It also crystallises from acetone/CH2Cl2/hexane (2:2:1) [Blau & Espenson J Am Chem Soc 108 1962 1986, White & Murray J Am Chem Soc 109 2576 1987]. [Beilstein 4 IV 332.]
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

Tetraethylammonium chloride monohydrate, 98+%(68696-18-4)
[Sigma Aldrich]

68696-18-4(sigmaaldrich)
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