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ChemicalBook--->CAS DataBase List--->1714-29-0

1714-29-0

1714-29-0 Structure

1714-29-0 Structure
IdentificationMore
[Name]

1-Bromopyrene
[CAS]

1714-29-0
[Synonyms]

1-BROMOPYRENE
Pyrene, 1-bromo-
2-Bromopyrene
1-Pyrenyl bromide
[EINECS(EC#)]

626-844-5
[Molecular Formula]

C16H9Br
[MDL Number]

MFCD00015767
[Molecular Weight]

281.15
[MOL File]

1714-29-0.mol
Chemical PropertiesBack Directory
[Melting point ]

102-105 °C (lit.)
[Boiling point ]

255 °C / 7mmHg
[density ]

1.4316 (rough estimate)
[refractive index ]

1.6000 (estimate)
[storage temp. ]

Keep in dark place,Sealed in dry,Room Temperature
[solubility ]

Chloroform (Soluble), DMSO (Slightly, Heated, Sonicated), Methanol (Slightly)
[form ]

Crystalline
[color ]

White to Pale Yellow
[InChIKey]

HYGLETVERPVXOS-UHFFFAOYSA-N
[CAS DataBase Reference]

1714-29-0(CAS DataBase Reference)
[NIST Chemistry Reference]

1-Bromopyrene(1714-29-0)
Safety DataBack Directory
[Hazard Codes ]

Xi
[Risk Statements ]

R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36:Wear suitable protective clothing .
[WGK Germany ]

3
[HS Code ]

29039990
Hazard InformationBack Directory
[Chemical Properties]

White to yellow to light brown powder
[Uses]

1-Bromopyrene is used in the cleavage of DNA in studies. It is also used in the preparation of DNA base analogs.
[Preparation]

1-Bromopyrene is an important intermediate in the OLED material industry. The synthesis method is as follows: pyrene is dissolved in an organic solvent dichloromethane, and dibromohydantoin is added for reaction, filtered, and the obtained solid is recrystallized to obtain 1-bromopyrene.
[Synthesis Reference(s)]

Synthetic Communications, 18, p. 2207, 1988 DOI: 10.1080/00397918808082362
[General Description]

1-Bromopyrene, a polycyclic aromatic hydrocarbon (PAH), is a mono bromo substituted pyrene derivative. Its synthesis has been reported. Its gas phase UV-absorption spectra in the UV wavelength range at elevated temperature has been studied. Electron affinitiy (EA) of 1-bromopyrene has been investigated using electron attachment desorption chemical ionization mass spectrometry (DCI-MS) and triple quadrupole tandem mass spectrometry. It participates in the synthesis of novel ruthenium (II) bipyridine or terpyridine complexes bearing pyrene moiety. The reaction of 1-bromopyrene cation radical with water in acetonitrile has been analyzed using the electron transfer stopped-flow (ETSF) method.
Spectrum DetailBack Directory
[Spectrum Detail]

1-Bromopyrene(1714-29-0)MS
1-Bromopyrene(1714-29-0)1HNMR
1-Bromopyrene(1714-29-0)13CNMR
1-Bromopyrene(1714-29-0)IR1
1-Bromopyrene(1714-29-0)IR2
1-Bromopyrene(1714-29-0)Raman
Well-known Reagent Company Product InformationBack Directory
[Alfa Aesar]

1-Bromopyrene, 95%(1714-29-0)
[Sigma Aldrich]

1714-29-0(sigmaaldrich)
[TCI AMERICA]

1-Bromopyrene,>94.0%(GC)(1714-29-0)
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