| Identification | More | [Name]
N-Acetylethylenediamine | [CAS]
1001-53-2 | [Synonyms]
N-(2-AMINOETHYL)ACETAMIDE
N-ACETYLETHYLENEDIAMINE
Acetamide, N-(2-aminoethyl-)
Acetamide, N-(2-aminoethyl)-
N-Monoacetylethylenediamine
N-ACETYLETHYLENEDIAMINE, TECH., 90%
2-(acetamido)ethylamine
2-(Acetamino)ethylamine
N-Acetylethylenediamine ,97%
N-Acetyl-1,2-ethanediamine | [Molecular Formula]
C4H10N2O | [MDL Number]
MFCD00008163 | [Molecular Weight]
102.14 | [MOL File]
1001-53-2.mol |
| Chemical Properties | Back Directory | [Appearance]
White to yellow crystalline solid | [Melting point ]
50 °C (lit.) | [Boiling point ]
128 °C/3 mmHg (lit.) | [density ]
1.066 g/cm3 at 25 °C(lit.)
| [refractive index ]
n20/D 1.485(lit.)
| [Fp ]
>230 °F
| [storage temp. ]
Keep in dark place,Inert atmosphere,Room temperature | [solubility ]
DMSO (Slightly), Methanol (Slightly) | [form ]
Solid | [pka]
15.97±0.46(Predicted) | [color ]
White to Yellow Low-Melting | [Sensitive ]
Hygroscopic | [Detection Methods]
T,NMR | [BRN ]
1743120 | [CAS DataBase Reference]
1001-53-2(CAS DataBase Reference) | [NIST Chemistry Reference]
N-Acetylethylenediamine(1001-53-2) | [Storage Precautions]
Store under nitrogen |
| Safety Data | Back Directory | [Risk Statements ]
R34:Causes burns. | [Safety Statements ]
S23:Do not breathe gas/fumes/vapor/spray (appropriate wording to be specified by the manufacturer) .
S24/25:Avoid contact with skin and eyes . | [RIDADR ]
3259 | [WGK Germany ]
3
| [F ]
3 | [HazardClass ]
8 | [PackingGroup ]
III | [HS Code ]
29241990 |
| Hazard Information | Back Directory | [Chemical Properties]
White to yellow crystalline solid | [Uses]
N-(2-Aminoethyl)acetamide may be used in the preparation of mixed two-component monolayers on glassy carbon. It may be used in the synthesis of lysidine. | [General Description]
N-(2-Aminoethyl)acetamide is an organic building block. | [Purification Methods]
The acetyl-diamine has been fractionated under reduced pressure and fraction b 125-130o/5mm was refractionated, fraction b 132-135o/4mm was collected and solidified. It is a low melting hygroscopic solid which can be recrystallised from dioxane/Et2O. It is soluble in H2O, Et2O and *C6H6. The p-toluenesulfonate salt can be recrystallised from EtOH/EtOAc (1:8), has m 125-126o but the free base cannot be recovered from it by basifying and extracting with CH2Cl2. The picrate has m 175o (from EtOH) [Aspinall J Am Chem Soc 63 853 1941, Hall J Am Chem Soc 78 2570 1956]. [Beilstein 4 IV 1193.] |
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