UDP-L-arabinose synthesis

1synthesis methods

Product Name:UDP-L-arabinose
CAS Number:15839-78-8
Molecular formula:C14H22N2O16P2
Molecular Weight:536.28

1-O,2-O,3-O,4-O-Tetrakis(trimethylsilyl)-β-L-arabinopyranose

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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: iodotrimethylsilane / CH₂Cl₂ / 0.5 h / 20 °C
2.1: CH₂Cl₂ / 4 h
2.2: tetrabutylammonium fluoride / CH₂Cl₂; tetrahydrofuran / 1 h
2.3: alkaline phosphatase / various solvent(s) / 16 h / 20 °C / pH 8

References:

Uchiyama, Taketo;Hindsgaul, Ole [Journal of Carbohydrate Chemistry,1998,vol. 17,# 8,p. 1181 - 1190]

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