TRIPHENYLACRYLONITRILE synthesis
- Product Name:TRIPHENYLACRYLONITRILE
- CAS Number:6304-33-2
- Molecular formula:C21H15N
- Molecular Weight:281.35
1607-57-4
169 suppliers
$10.00/1g
105-56-6
442 suppliers
$10.00/5ml
6304-33-2
28 suppliers
$58.79/5g
Yield:6304-33-2 81%
Reaction Conditions:
Stage #1: Triphenylvinyl bromidewith copper(I) oxide;oxygen;triphenylphosphine in 1-methyl-pyrrolidin-2-one;Schlenk technique;Sealed tube;
Stage #2: ethyl 2-cyanoacetatewith silver nitrate;acetic acid in 1-methyl-pyrrolidin-2-one at 130; for 18 h;Schlenk technique;Sealed tube;
References:
Wang, Xian-Jin;Zhang, Song-Lin [New Journal of Chemistry,2017,vol. 41,# 24,p. 14826 - 14830] Location in patent:supporting information
1607-57-4
169 suppliers
$10.00/1g
6304-33-2
28 suppliers
$58.79/5g
140-29-4
5 suppliers
$21.00/25mL
6304-33-2
28 suppliers
$58.79/5g
5350-66-3
1 suppliers
inquiry
6304-33-2
28 suppliers
$58.79/5g