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ChemicalBook CAS DataBase List trimethyl((tetrahydro-2H-pyran-4-yl)ethynyl)silane
1604039-54-4

trimethyl((tetrahydro-2H-pyran-4-yl)ethynyl)silane synthesis

6synthesis methods
25637-18-7 Synthesis
4-IODOTETRAHYDRO-2H-PYRAN

25637-18-7
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$6.00/250mg

61210-52-4 Synthesis
trimethylsilylethynylmagnesium bromide

61210-52-4
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trimethyl((tetrahydro-2H-pyran-4-yl)ethynyl)silane

1604039-54-4
19 suppliers
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Yield:1604039-54-4 82%

Reaction Conditions:

with iron(II) bromide in tetrahydrofuran;1-methyl-pyrrolidin-2-one at 20; for 16 h;Inert atmosphere;Glovebox;

References:

Cheung, Chi Wai;Ren, Peng;Hu, Xile [Organic Letters,2014,vol. 16,# 9,p. 2566 - 2569] Location in patent:supporting information

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