TRIETHYLPHOSPHONODIFLUOROACETATE synthesis
- Product Name:TRIETHYLPHOSPHONODIFLUOROACETATE
- CAS Number:17843-01-5
- Molecular formula:
- Molecular Weight:0
867-13-0
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17843-01-5
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Yield:17843-01-5 69%
Reaction Conditions:
Stage #1: diethoxyphosphoryl-acetic acid ethyl esterwith sodium hydride in tetrahydrofuran at 0 - 20; for 2 h;
Stage #2: with Selectfluor in tetrahydrofuran at 0 - 20; for 4 h;
References:
Marma, Mong S.;Khawli, Leslie A.;Harutunian, Vahak;Kashemirov, Boris A.;McKenna, Charles E. [Journal of Fluorine Chemistry,2005,vol. 126,# 11-12,p. 1467 - 1475]
2356-16-3
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17843-01-5
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1478-53-1
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$16.00/500mg
541-41-3
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$21.00/5g
17843-01-5
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78715-58-9
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110624-88-9
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