TRIETHYLENE GLYCOL MONOMETHYL ETHER synthesis
- Product Name:TRIETHYLENE GLYCOL MONOMETHYL ETHER
- CAS Number:112-35-6
- Molecular formula:C7H16O4
- Molecular Weight:164.2
Yield:13826-35-2 87%
Steps:
1 EXAMPLE 1
The analysis indicated that the conversion of m-hydroxybenzyl alcohol was 99%, the yield of m-phenoxybenzyl alcohol was 93%, and the residue percentage of triethylene glycol monomethyl ether was 98% relative to the charged amount. The combined solution was also subjected to vacuum distillation, and there were recovered chlorobenzene and 162.5 g (purity: 98%, recovery: 97%) of triethylene glycol monomethyl ether, and there was obtained 71.6 g purity: 98%, isolation yield: 87%) of pure m-phenoxybenzyl alcohol.
References:
US5068459,1991,A
249508-40-5
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