Triethoxyoctylsilane synthesis
- Product Name:Triethoxyoctylsilane
- CAS Number:2943-75-1
- Molecular formula:C14H32O3Si
- Molecular Weight:276.49
111-66-0
164 suppliers
$10.00/10ml
998-30-1
251 suppliers
$30.00/25g
2943-75-1
339 suppliers
$8.00/25g
Yield:2943-75-1 100%
Reaction Conditions:
at 90; for 5 h;Inert atmosphere;
Steps:
11 Example 11
In a 500-ml three-necked flask, octene (1.25 mol) was added, and Catalyst 1 (1.25 mmol) prepared in Example 1 was slowly heated to 90°C under a nitrogen atmosphere.While stirring, triethoxyhydrosilane (1.5 mol) was added dropwise through the dropping funnel. The dropwise addition time was 0.5 hours, the reaction temperature was maintained, and the stirring reaction was continued for 5 hours.After cooling to room temperature, the corresponding fractions were collected by distillation under reduced pressure. The conversion of octene was 94.7% as determined by GC-MS.The yield of the β adduct 1-triethoxysilyloctane was 100%.
References:
CN107857776,2018,A Location in patent:Paragraph 0048; 0049
111-66-0
164 suppliers
$10.00/10ml
998-30-1
251 suppliers
$30.00/25g
78-10-4
432 suppliers
$12.00/25g
2943-75-1
339 suppliers
$8.00/25g
111-66-0
164 suppliers
$10.00/10ml
998-30-1
251 suppliers
$30.00/25g
78-10-4
432 suppliers
$12.00/25g
2157-42-8
6 suppliers
inquiry
2943-75-1
339 suppliers
$8.00/25g
111-66-0
164 suppliers
$10.00/10ml
998-30-1
251 suppliers
$30.00/25g
2943-75-1
339 suppliers
$8.00/25g
911808-73-6
0 suppliers
inquiry
111-66-0
164 suppliers
$10.00/10ml
998-30-1
251 suppliers
$30.00/25g
111-65-9
276 suppliers
$12.00/25g
2943-75-1
339 suppliers
$8.00/25g