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ChemicalBook CAS DataBase List Tetrathiophen-2-yl-silane
17940-73-7

Tetrathiophen-2-yl-silane synthesis

5synthesis methods
188290-36-0 Synthesis
Thiophene(SIV) (9CI)

188290-36-0
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Yield:17940-73-7 70%

Reaction Conditions:

Stage #1: thiophenewith n-butyllithium in tetrahydrofuran;hexane at -70;
Stage #2: with tetramethylorthosilicate in hexane;

References:

Gontarczyk, Krzysztof;Durka, Krzysztof;Klimkowski, Piotr;Luliński, Sergiusz;Serwatowski, Janusz;Wo?niak, Krzysztof [Journal of Organometallic Chemistry,2015,vol. 783,p. 1 - 9]