TETRAPHENYLANTIMONY BROMIDE synthesis
- Product Name:TETRAPHENYLANTIMONY BROMIDE
- CAS Number:21450-52-2
- Molecular formula:C24H20BrSb
- Molecular Weight:510.08
Yield:21450-52-2 54.4%
Reaction Conditions:
with HBr in diethyl ether;toluene;slow addn. of a suspn. of Ph3SbCl2 in ether/toluene (2/1 v/v) to a soln.of PhMgBr in ether under stirring; soln. was allowed to stand at room t emp. for 6 d with occasional stirring; slow addn. of ice and 40% HBr under stirring; mixt. stirred overnight; ppt. was filtered off and recrystd. from water/ethanol (3/2);
References:
Ma, Yongqiang;Li, Jinshan;Xuan, Zhenai;Liu, Runchang [Journal of Organometallic Chemistry,2001,vol. 620,# 1-2,p. 235 - 242]
603-36-1
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21450-52-2
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