TETRAHYDROPIPERINE synthesis
- Product Name:TETRAHYDROPIPERINE
- CAS Number:23434-88-0
- Molecular formula:C17H23NO3
- Molecular Weight:289.37
110-89-4
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23434-88-0
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$25.00/1mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: sodium methylate / toluene / 1 h / 55 °C / Inert atmosphere
1.2: 55 - 60 °C / Inert atmosphere
2.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / dimethyl sulfoxide; water / 25 - 30 °C
3.1: palladium 10% on activated carbon; hydrogen / methanol / 40 - 45 °C / 2068.65 - 2585.81 Torr
References:
CIPLA LIMITED;PHULL, Manjinder Singh;RAO, Dharmaraj Ramachandra;MALHOTRA, Geena;BIRARI, Dilip Ramdas;DESAI, Sachin Vasant WO2019/73491, 2019, A1
94-62-2
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23434-88-0
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23512-46-1
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$247.00/1mg
23434-88-0
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41917-45-7
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23434-88-0
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50838-22-7
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23434-88-0
106 suppliers
$25.00/1mg